triphenylphosphoniumbromid

Base Information

Chemical Name:triphenylphosphoniumbromid
CAS No.:102235-89-2
Molecular Formula:Br*C₂₇H₂₅NOP
Molecular Weight:490.379
Hs Code.:

<N-Methyl-N-phenylcarbamoylmethyl>triphenylphosphoniumbromid

Synonyms:triphenylphosphoniumbromid

Suppliers and Price of triphenylphosphoniumbromid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylphosphoniumbromid

Chemical Property:

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Technology Process of triphenylphosphoniumbromid

There total 2 articles about triphenylphosphoniumbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 29182-97-6
N-methyl-2-bromoacetanilide

: 603-35-0
triphenylphosphine

: 102235-89-2
triphenylphosphoniumbromid

Guidance literature:: In toluene; for 12h; Ambient temperature;

Reference yield:

: 100-61-8
N-methylaniline

: 102235-89-2
triphenylphosphoniumbromid

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Et₃N/pyridine / toluene / Ambient temperature

2: 82 percent / toluene / 12 h / Ambient temperature

With pyridine; triethylamine; In toluene;

Reference yield: 90.0%

: 54322-65-5
cyclopropylacetyl chloride

: 102235-89-2
triphenylphosphoniumbromid

: 1432498-53-7
N-methyl-N-phenyl-4-cyclopropyl-2,3-butadienamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ja4025963