C₁₇H₂₂N₄O₂S

Base Information

Chemical Name:C₁₇H₂₂N₄O₂S
CAS No.:1374991-76-0
Molecular Formula:C₁₇H₂₂N₄O₂S
Molecular Weight:346.453
Hs Code.:

C<sub>17</sub>H<sub>22</sub>N<sub>4</sub>O<sub>2</sub>S

Synonyms:C₁₇H₂₂N₄O₂S

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Chemical Property of C₁₇H₂₂N₄O₂S

Chemical Property:

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Technology Process of C₁₇H₂₂N₄O₂S

There total 12 articles about C₁₇H₂₂N₄O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374991-67-9
(6S,7S)-6-(methoxymethoxy)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecane

: 1374991-76-0
C₁₇H₂₂N₄O₂S

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / methanol / 0.5 h / 15 °C / Cooling with ice

2.1: dmap; triethylamine / dichloromethane / 3 h / 20 °C / Cooling with ice

3.1: sodium hydrogencarbonate; sodium iodide / acetone / 3 h / Reflux

4.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexane / 0.83 h / -50 °C / Inert atmosphere

4.2: 3 h / -50 - 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 - 20 °C

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; n-butyllithium; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; sodium iodide; In tetrahydrofuran; methanol; hexane; dichloromethane; acetone; 6.1: Mitsunobu reaction;
DOI:10.1016/j.tetasy.2012.03.005

Reference yield:

: 1374991-68-0
(2S,3S)-4-(tert-butyldiphenylsilyloxy)-3-(methoxymethoxy)-2-methylbutyl 4-methylbenzenesulfonate

: 1374991-76-0
C₁₇H₂₂N₄O₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate; sodium iodide / acetone / 3 h / Reflux

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexane / 0.83 h / -50 °C / Inert atmosphere

2.2: 3 h / -50 - 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 - 20 °C

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; triphenylphosphine; sodium iodide; In tetrahydrofuran; hexane; acetone; 4.1: Mitsunobu reaction;
DOI:10.1016/j.tetasy.2012.03.005

Reference yield:

: 1374991-69-1
(S)-5-((S)-hex-4-yn-2-yl)-9,9-dimethyl-8,8-diphenyl-2,4,7-trioxa-8-siladecane

: 1374991-76-0
C₁₇H₂₂N₄O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 - 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; triphenylphosphine; In tetrahydrofuran; 2: Mitsunobu reaction;
DOI:10.1016/j.tetasy.2012.03.005