phenylmethyl 2-O-acetyl-6-deoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-3-O-methyl-α-L-mannopyranoside

Base Information

Chemical Name:phenylmethyl 2-O-acetyl-6-deoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-3-O-methyl-α-L-mannopyranoside
CAS No.:168567-04-2
Molecular Formula:C₂₂H₃₆O₆Si
Molecular Weight:424.61
Hs Code.:

Synonyms:phenylmethyl 2-O-acetyl-6-deoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-3-O-methyl-α-L-mannopyranoside

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Chemical Property of phenylmethyl 2-O-acetyl-6-deoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-3-O-methyl-α-L-mannopyranoside

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Technology Process of phenylmethyl 2-O-acetyl-6-deoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-3-O-methyl-α-L-mannopyranoside

There total 9 articles about phenylmethyl 2-O-acetyl-6-deoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-3-O-methyl-α-L-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 108-24-7
acetic anhydride

: 138785-32-7
phenylmethyl 6-deoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-3-O-methyl-α-L-mannopyranoside

: 168567-04-2
phenylmethyl 2-O-acetyl-6-deoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-3-O-methyl-α-L-mannopyranoside

Guidance literature:: With pyridine;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 168567-04-2
phenylmethyl 2-O-acetyl-6-deoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-3-O-methyl-α-L-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / imidazole / CH₂Cl₂

2: 96 percent / OsO₄, NMO / acetone; H₂O

3: 1.) Bu₂SnO, 2.) TBAB / 1,) MeOH, 2.) PhH

4: pyridine

With pyridine; 1H-imidazole; osmium(VIII) oxide; N-methyl-2-indolinone; tetrabutylammomium bromide; di(n-butyl)tin oxide; In dichloromethane; water; acetone;
DOI:10.1021/jo951560x

Reference yield:

: 76404-30-3
Benzyl-2,3,6-tridesoxy-α-L-erythro-hex-2-enopyranosid

: 168567-04-2
phenylmethyl 2-O-acetyl-6-deoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-3-O-methyl-α-L-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / imidazole / CH₂Cl₂

2: 96 percent / OsO₄, NMO / acetone; H₂O

3: 1.) Bu₂SnO, 2.) TBAB / 1,) MeOH, 2.) PhH

4: pyridine

With pyridine; 1H-imidazole; osmium(VIII) oxide; N-methyl-2-indolinone; tetrabutylammomium bromide; di(n-butyl)tin oxide; In dichloromethane; water; acetone;
DOI:10.1021/jo951560x