DL-2-acetamido-4-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitro-1-phenoxy]butanoic acidd

Base Information

Chemical Name:DL-2-acetamido-4-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitro-1-phenoxy]butanoic acidd
CAS No.:338735-82-3
Molecular Formula:C₁₄H₁₃F₃N₄O₆
Molecular Weight:390.276
Hs Code.:

Synonyms:DL-2-acetamido-4-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitro-1-phenoxy]butanoic acidd

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of DL-2-acetamido-4-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitro-1-phenoxy]butanoic acidd

Chemical Property:

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Technology Process of DL-2-acetamido-4-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitro-1-phenoxy]butanoic acidd

There total 3 articles about DL-2-acetamido-4-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitro-1-phenoxy]butanoic acidd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 338735-80-1
2-acetylamino-2-{2-[2-nitro-4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenoxy]-ethyl}-malonic acid

: 338735-82-3
DL-2-acetamido-4-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitro-1-phenoxy]butanoic acidd

Guidance literature:: In 1,4-dioxane; at 80 ℃; for 1h;
DOI:10.3987/com-00-s(i)90

Reference yield:

: 271252-28-9
4-(1-azi-2,2,2-trifluoroethyl)-1-(2-bromoethoxy)-2-nitrobenzene

: 338735-82-3
DL-2-acetamido-4-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitro-1-phenoxy]butanoic acidd

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / KH / dimethylformamide / 24 h / -42 - 20 °C

2: 84 percent / aq. NaOH / ethanol; H₂O / 20 °C

3: dioxane / 1 h / 80 °C

With sodium hydroxide; potassium hydride; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.3987/com-00-s(i)90

Reference yield:

: 338735-79-8
diethyl acetamido[2-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitro-1-phenoxy]ethyl]malonate

: 338735-82-3
DL-2-acetamido-4-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitro-1-phenoxy]butanoic acidd

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / aq. NaOH / ethanol; H₂O / 20 °C

2: dioxane / 1 h / 80 °C

With sodium hydroxide; In 1,4-dioxane; ethanol; water;
DOI:10.3987/com-00-s(i)90