1-Chloro-4-(ethylsulfonyl)-2-nitrobenzene

Base Information

Chemical Name:1-Chloro-4-(ethylsulfonyl)-2-nitrobenzene
CAS No.:74159-80-1
Molecular Formula:C8H8ClNO4S
Molecular Weight:249.675
Hs Code.:2904909090
European Community (EC) Number:277-737-1
DSSTox Substance ID:DTXSID50995598
Nikkaji Number:J318.917A
Wikidata:Q72450309
Mol file:74159-80-1.mol

Synonyms:1-chloro-4-(ethylsulfonyl)-2-nitrobenzene;74159-80-1;1-chloro-4-ethylsulfonyl-2-nitrobenzene;2-NITRO-4-ETHYLSULFONYL CHLOROBENZENE;1-Chloro-4-(ethylsulphonyl)-2-nitrobenzene;EINECS 277-737-1;1-CHLORO-4-(ETHANESULFONYL)-2-NITROBENZENE;ethyl 4-chloro-3-nitrophenyl sulphone;SCHEMBL3209835;DTXSID50995598;STK663477;4-Chloro-3-nitrophenyl ethyl sulfone;AKOS003292649;CS-0331176;FT-0650118;W-104429

Suppliers and Price of 1-Chloro-4-(ethylsulfonyl)-2-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-Chloro-4-(ethylsulfonyl)-2-nitrobenzene 95+%
1g
$ 455.00

Alichem
1-Chloro-4-(ethylsulfonyl)-2-nitrobenzene
1g
$ 409.20

Total 42 raw suppliers

Chemical Property of 1-Chloro-4-(ethylsulfonyl)-2-nitrobenzene

Chemical Property:

Vapor Pressure:7.32E-07mmHg at 25°C
Refractive Index:1.562
Boiling Point:419.6 °C at 760 mmHg
Flash Point:207.6 °C
PSA：88.34000
Density:1.455 g/cm³
LogP:3.64580
Storage Temp.:2-8°C
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:248.9862566
Heavy Atom Count:15
Complexity:332

Purity/Quality:

99% ^*data from raw suppliers

1-Chloro-4-(ethylsulfonyl)-2-nitrobenzene 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCS(=O)(=O)C1=CC(=C(C=C1)Cl)[N+](=O)[O-]

Technology Process of 1-Chloro-4-(ethylsulfonyl)-2-nitrobenzene

There total 4 articles about 1-Chloro-4-(ethylsulfonyl)-2-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 7205-80-3
1-(ethylsulfonyl)-4-chlorobenzene

: 74159-80-1
1-chloro-4-(ethylsulphonyl)-2-nitrobenzene

Guidance literature:: With sulfuric acid; potassium nitrate; at 80 - 90 ℃;
DOI:10.1111/j.1747-0285.2012.01442.x

Reference yield:

: 98-60-2
4-chlorobenzenesulfonyl chloride

: 74159-80-1
1-chloro-4-(ethylsulphonyl)-2-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; tellurium; rongalite / tetrahydrofuran; water / 0.08 h / 20 °C / Inert atmosphere

1.2: 5 h / 90 °C / Inert atmosphere

2.1: sulfuric acid; potassium nitrate / 80 - 90 °C

With tellurium; sulfuric acid; N-benzyl-N,N,N-triethylammonium chloride; rongalite; potassium nitrate; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1111/j.1747-0285.2012.01442.x

Reference yield:

: 5120-72-9
p-chlorophenyl ethyl sulfide

: 74159-80-1
1-chloro-4-(ethylsulphonyl)-2-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; sodium tungstate (VI) dihydrate / ethyl acetate / 5 h / 30 - 55 °C / Large scale

2: nitric acid; sulfuric acid / 2 h / 0 - 20 °C / Large scale

With sodium tungstate (VI) dihydrate; sulfuric acid; dihydrogen peroxide; nitric acid; In ethyl acetate;