trans-N-methyl-N-phenethyl-2-[4-benzyloxy-3-(2carbomethoxyvinyl)phenyl]acetamide

Base Information

Chemical Name:trans-N-methyl-N-phenethyl-2-[4-benzyloxy-3-(2carbomethoxyvinyl)phenyl]acetamide
CAS No.:142588-45-2
Molecular Formula:C₂₈H₂₉NO₄
Molecular Weight:443.543
Hs Code.:

Synonyms:trans-N-methyl-N-phenethyl-2-[4-benzyloxy-3-(2carbomethoxyvinyl)phenyl]acetamide

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Chemical Property of trans-N-methyl-N-phenethyl-2-[4-benzyloxy-3-(2carbomethoxyvinyl)phenyl]acetamide

Chemical Property:

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Technology Process of trans-N-methyl-N-phenethyl-2-[4-benzyloxy-3-(2carbomethoxyvinyl)phenyl]acetamide

There total 8 articles about trans-N-methyl-N-phenethyl-2-[4-benzyloxy-3-(2carbomethoxyvinyl)phenyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142588-49-6
(Z)-3-{2-Benzyloxy-5-[(methyl-phenethyl-carbamoyl)-methyl]-phenyl}-acrylic acid methyl ester

: 142588-45-2
trans-N-methyl-N-phenethyl-2-[4-benzyloxy-3-(2carbomethoxyvinyl)phenyl]acetamide

Guidance literature:: With iodine; In chloroform; for 12h; Heating;
DOI:10.1021/jm9506985

Reference yield:

: 100-39-0
benzyl bromide

: 142588-45-2
trans-N-methyl-N-phenethyl-2-[4-benzyloxy-3-(2carbomethoxyvinyl)phenyl]acetamide

Guidance literature:: Multi-step reaction with 6 steps

1: aq. NaOH / ethanol / 3 h / Heating

2: 94 percent / HCl / 3 h / Ambient temperature

3: aq. LiOH / tetrahydrofuran; methanol / 12 h / Ambient temperature

4: CH₂Cl₂ / 0.33 h / Ambient temperature

5: CH₂Cl₂ / 8 h

6: I₂ / CHCl₃ / 12 h / Heating

With hydrogenchloride; lithium hydroxide; sodium hydroxide; iodine; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform;
DOI:10.1021/jm9506985

Reference yield:

: 1027297-23-9
(Z)-3-(5-Carboxymethyl-2-hydroxy-phenyl)-acrylic acid

: 142588-45-2
trans-N-methyl-N-phenethyl-2-[4-benzyloxy-3-(2carbomethoxyvinyl)phenyl]acetamide

Guidance literature:: Multi-step reaction with 6 steps

1: aq. NaOH / ethanol / 3 h / Heating

2: 94 percent / HCl / 3 h / Ambient temperature

3: aq. LiOH / tetrahydrofuran; methanol / 12 h / Ambient temperature

4: CH₂Cl₂ / 0.33 h / Ambient temperature

5: CH₂Cl₂ / 8 h

6: I₂ / CHCl₃ / 12 h / Heating

With hydrogenchloride; lithium hydroxide; sodium hydroxide; iodine; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform;
DOI:10.1021/jm9506985