4-Chloro-3',4'-dimethylbenzophenone

Base Information

• Chemical Name: 4-Chloro-3',4'-dimethylbenzophenone
• CAS No.: 40415-10-9
• Molecular Formula: C₁₅H₁₃ClO
• Molecular Weight: 244.721
• DSSTox Substance ID: DTXSID50373913
• Wikidata: Q82162310
• Mol file: 40415-10-9.mol

Synonyms:4-Chloro-3',4'-dimethylbenzophenone;40415-10-9;(4-chlorophenyl)-(3,4-dimethylphenyl)methanone;SCHEMBL11278601;DTXSID50373913;YMDVVGLPIKIHRX-UHFFFAOYSA-N;4'-chloro-3,4-dimethylbenzophenone;MFCD06201507;AKOS009339235;A821531;(4-Chloro-phenyl)-(3,4-dimethyl-phenyl)-methanone

Chemical Property of 4-Chloro-3',4'-dimethylbenzophenone

Chemical Property:

• Vapor Pressure: 4.04E-06mmHg at 25°C
• XLogP3: 5.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 244.0654927
• Heavy Atom Count: 17
• Complexity: 268

Purity/Quality:

98% ^*data from raw suppliers

4-Chloro-3',4'-dimethylbenzophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=C(C=C(C=C1)C(=O)C2=CC=C(C=C2)Cl)C

Technology Process of 4-Chloro-3',4'-dimethylbenzophenone

There total 2 articles about 4-Chloro-3',4'-dimethylbenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

4-(4-chlorobenzyl)-1,2-dimethyl-benzene → (4-chlorophenyl)(3,4-dimethylphenyl)methanone (40415-10-9)

Guidance literature:

With oxygen; sodium t-butanolate; In dimethyl sulfoxide; at 50 ℃; for 5h; Sealed tube;

DOI:10.1055/s-0036-1588928

Reference yield: 89.0%

→ (4-chlorophenyl)(3,4-dimethylphenyl)methanone (40415-10-9)

Guidance literature:

With oxygen; sodium t-butanolate; In dimethyl sulfoxide; at 50 ℃; for 5h;

Refernces

• 1、 Li, Jiang-Sheng,Yang, Fan,Yang, Qian,Li, Zhi-Wei,Chen, Guo-Qin,Da, Yu-Dong,Huang, Peng-Mian,Chen, Chao,Zhang, Yuefei,Huang, Ling-Zhi. "T-BuONa-Mediated Transition-Metal-Free Autoxidation of Diarylmethanes to Ketones". supporting information. p. 994 - 998. Retrieved 2017/05/10.