Technology Process of C16H16O3S
There total 5 articles about C16H16O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(l) iodide; sodium t-butanolate;
In
toluene;
Heating;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: H2 / Pd/C / methanol / 5 h / 45 °C
2: NaNO2; HCl; KI / H2O / 20 h / -5 - 20 °C
3: 95 percent / neuocuprine; CuI; NaOtBu / toluene / Heating
With
hydrogenchloride; copper(l) iodide; hydrogen; potassium iodide; sodium t-butanolate; sodium nitrite;
palladium on activated charcoal;
In
methanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / dimethylformamide / 20 °C
1.2: 80 percent / H2O2; aq. NaOH / cooling
2.1: 100 percent / diethyl ether / 20 °C
3.1: H2 / Pd/C / methanol / 5 h / 45 °C
4.1: NaNO2; HCl; KI / H2O / 20 h / -5 - 20 °C
5.1: 95 percent / neuocuprine; CuI; NaOtBu / toluene / Heating
With
hydrogenchloride; copper(l) iodide; hydrogen; sodium hydride; potassium iodide; sodium t-butanolate; sodium nitrite;
palladium on activated charcoal;
In
methanol; diethyl ether; water; N,N-dimethyl-formamide; toluene;