3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(((trifluoromethyl)sulfonyl)oxy)isophthalate

Base Information

Chemical Name:3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(((trifluoromethyl)sulfonyl)oxy)isophthalate
CAS No.:1201221-81-9
Molecular Formula:C₁₈H₂₅F₃O₇SSi
Molecular Weight:470.539
Hs Code.:

Synonyms:3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(((trifluoromethyl)sulfonyl)oxy)isophthalate

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Chemical Property of 3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(((trifluoromethyl)sulfonyl)oxy)isophthalate

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Technology Process of 3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(((trifluoromethyl)sulfonyl)oxy)isophthalate

There total 5 articles about 3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(((trifluoromethyl)sulfonyl)oxy)isophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-hydroxyisophthalate

: 1201221-81-9
3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(((trifluoromethyl)sulfonyl)oxy)isophthalate

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 0.5h;

Reference yield: 91.0%

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 431049-88-6
C₁₃H₁₃F₃O₇S

: 1201221-81-9
3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(((trifluoromethyl)sulfonyl)oxy)isophthalate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 18h;
DOI:10.1016/j.bmcl.2009.08.100

Reference yield:

: 576170-38-2
3-(tert-butyl) 1-methyl 4-hydroxyisophthalate

: 1201221-81-9
3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(((trifluoromethyl)sulfonyl)oxy)isophthalate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / toluene / 0.92 h / 0 - 20 °C

1.2: 0.5 h / 50 °C

2.1: pyridine / dichloromethane / 0.5 h / 0 - 20 °C

With pyridine; sodium hydride; In dichloromethane; toluene;