3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalate

Base Information

Chemical Name:3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalate
CAS No.:1201221-82-0
Molecular Formula:C₂₃H₃₇BO₆Si
Molecular Weight:448.44
Hs Code.:

Synonyms:3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalate

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Chemical Property of 3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalate

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Technology Process of 3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalate

There total 5 articles about 3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1201221-81-9
3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(((trifluoromethyl)sulfonyl)oxy)isophthalate

: 73183-34-3
bis(pinacol)diborane

: 1201221-82-0
3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalate

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 65 ℃; for 3h;

Reference yield:

: 576170-38-2
3-(tert-butyl) 1-methyl 4-hydroxyisophthalate

: 1201221-82-0
3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / toluene / 0.92 h / 0 - 20 °C

1.2: 0.5 h / 50 °C

2.1: pyridine / dichloromethane / 0.5 h / 0 - 20 °C

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 3 h / 65 °C

With pyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; sodium hydride; In 1,4-dioxane; dichloromethane; toluene;

Reference yield:

: 3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-hydroxyisophthalate

: 1201221-82-0
3-tert-butyl 1-(2-(trimethylsilyl)ethyl) 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0.5 h / 0 - 20 °C

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 3 h / 65 °C

With pyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; dichloromethane;