2-OXO-2-PHENYLETHYL 4-AMINOBENZOATE

Base Information

• Chemical Name: 2-OXO-2-PHENYLETHYL 4-AMINOBENZOATE
• CAS No.: 107692-58-0
• Molecular Formula: C₁₅H₁₃NO₃
• Molecular Weight: 255.273
• Mol file: 107692-58-0.mol

Synonyms:4-Amino-benzoic acid 2-oxo-2-phenyl-ethyl ester

Chemical Property of 2-OXO-2-PHENYLETHYL 4-AMINOBENZOATE

Chemical Property:

• Boiling Point: 482.7±25.0 °C(Predicted)
• PKA: 2.05±0.10(Predicted)
• Density: 1.242±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

2-OXO-2-PHENYLETHYL 4-AMINOBENZOATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-OXO-2-PHENYLETHYL 4-AMINOBENZOATE

There total 1 articles about 2-OXO-2-PHENYLETHYL 4-AMINOBENZOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) + α-bromoacetophenone (70-11-1) → 4-Amino-benzoic acid 2-oxo-2-phenyl-ethyl ester (107692-58-0)

Guidance literature:

With potassium carbonate; In acetonitrile; room temperature, 20 min -> reflux, 50 min;

Reference yield: 83.0%

4-Amino-benzoic acid 2-oxo-2-phenyl-ethyl ester (107692-58-0) → 4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1)

Guidance literature:

With sodium hydrogen telluride; In N,N-dimethyl-formamide; for 0.333333h; Ambient temperature;

upstream raw materials:

4-amino-benzoic acid

α-bromoacetophenone

Downstream raw materials:

4-amino-benzoic acid

Refernces

• 1、 Pillay, M. Krishna,Kannan, K.,Ramasubramanian, P.. "KINETICS OF REACTION OF TRIETHYLAMMONIUM CARBOXYLATES WITH α-HALOGENOCARBONYL COMPOUNDS IN ORGANIC SOLVENTS. REACTION OF BENZOATES AND PHENOXYACETATES WITH PHENACYL BROMIDE IN ACETONE". . p. 3899 - 3908. Retrieved 2007/10/02.