4-vinylbenzyl methyl sulfide

Base Information

• Chemical Name: 4-vinylbenzyl methyl sulfide
• CAS No.: 15325-49-2
• Molecular Formula: C₁₀H₁₂S
• Molecular Weight: 164.271
• Mol file: 15325-49-2.mol

Synonyms:4-vinylbenzyl methyl sulfide

Chemical Property of 4-vinylbenzyl methyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-vinylbenzyl methyl sulfide

There total 2 articles about 4-vinylbenzyl methyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-Vinylbenzyl chloride (1592-20-7,29296-32-0) + sodium thiomethoxide (5188-07-8) → 4-vinylbenzyl methyl sulfide (15325-49-2)

Guidance literature:

In tetrahydrofuran; at 23 ℃; for 20h;

DOI:10.1002/pola.28359

Reference yield:

→ 4-vinylbenzyl methyl sulfide (15325-49-2)

Guidance literature:

p-Chlorstyrol, DMSO, Mg, THF;

Reference yield: 67.0%

1,3-propanesultone (1120-71-4) + 4-vinylbenzyl methyl sulfide (15325-49-2) → 3-(4-vinylbenzyl methyl sulfonio)propane-1-sulfonate

Guidance literature:

With 2,6-di-tert-butyl-4-methyl-phenol; In acetonitrile; at 50 ℃; for 67h;

DOI:10.1002/pola.28359

upstream raw materials:

4-Vinylbenzyl chloride

sodium thiomethoxide

Downstream raw materials:

1-(azidomethyl)-4-vinylbenzene

Refernces

• 1、 Liou, Ying-Shian,Tsai, Hsin-Chih,Yeh, Cheng-Yang,Tsiang, Raymond Chien-Chao. "Polymeric nanocomposite comprising gold nanoparticles and bilaterally sulfur-functionalized polystyrene". . p. 1268 - 1277. Retrieved 2015.