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Technology Process of C6H5(SbSC3H2(C6H5)2)

C6H5(SbSC3H2(C6H5)2)

Base Information
  • Chemical Name:C6H5(SbSC3H2(C6H5)2)
  • CAS No.:122115-79-1
  • Molecular Formula:C21H17SSb
  • Molecular Weight:423.182
  • Hs Code.:
C<sub>6</sub>H<sub>5</sub>(SbSC<sub>3</sub>H<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2)

Synonyms:C6H5(SbSC3H2(C6H5)2)

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Chemical Property of C6H5(SbSC3H2(C6H5)2)
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Technology Process of C6H5(SbSC3H2(C6H5)2)

There total 2 articles about C6H5(SbSC3H2(C6H5)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(C<sub>5</sub>H<sub>5</sub>)2(ZrSC<sub>3</sub>H<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2)

(C5H5)2(ZrSC3H2(C6H5)2)

dichlorophenylstibine
5035-52-9

dichlorophenylstibine

zirconocene dichloride
1291-32-3

zirconocene dichloride

C<sub>6</sub>H<sub>5</sub>(SbSC<sub>3</sub>H<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2)
122115-79-1

C6H5(SbSC3H2(C6H5)2)

Guidance literature:
In benzene; treatment of the Zr compd. in benzene suspn. with PhSbCl2 (1 equiv) (25°C), removal of solvent (vac.); extn. (hexane/ether (10:1)), chromy. (alumina III);
DOI:10.1021/om00110a049

Reference yield: 85.0%

(C<sub>5</sub>H<sub>5</sub>)2(ZrSC<sub>3</sub>H<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2)

(C5H5)2(ZrSC3H2(C6H5)2)

C<sub>6</sub>H<sub>5</sub>(SbSC<sub>3</sub>H<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2)
122115-79-1

C6H5(SbSC3H2(C6H5)2)

Guidance literature:
With C6H5SbCl2 or; C6H5SbBr2; In benzene; byproducts: Cp2ZrCl2 or, Cp2ZrBr2; room temp., according to Buchwald, S. L.; Fisher, R. A.; Davis, W. M. Organometallics 1989, 8, 2082.;
DOI:10.1021/ja00001a024
upstream raw materials:

dichlorophenylstibine

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