C₁₆H₁₈O₆

Base Information

Chemical Name:C₁₆H₁₈O₆
CAS No.:1419179-04-6
Molecular Formula:C₁₆H₁₈O₆
Molecular Weight:306.315
Hs Code.:

C<sub>16</sub>H<sub>18</sub>O<sub>6</sub>

Synonyms:C₁₆H₁₈O₆

Suppliers and Price of C₁₆H₁₈O₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₆H₁₈O₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₆H₁₈O₆

There total 1 articles about C₁₆H₁₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.3%

: 66323-03-3
4,5-bis(hydroxy)phthalic acid dimethyl ester

: 106-95-6
allyl bromide

: 1419178-82-7
C₁₃H₁₄O₆

: 1419179-04-6
C₁₆H₁₈O₆

Guidance literature:: With potassium carbonate; In acetone; for 6h; Inert atmosphere; Reflux;
DOI:10.1021/jo302353g

Reference yield: 60.2%

: 1419179-04-6
C₁₆H₁₈O₆

: 1419178-82-7
C₁₃H₁₄O₆

Guidance literature:: With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo302353g

Reference yield:

: 1419179-04-6
C₁₆H₁₈O₆

: 1419178-84-9
C₃₀H₄₂O₈

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium tetrahydroborate / ethanol / 2 h / 0 °C / Inert atmosphere

2: caesium carbonate / acetone / 4 h / Inert atmosphere; Reflux

3: chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 3 h / 0 °C / Inert atmosphere; Reflux

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol / 3 h / Inert atmosphere; Reflux

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate; caesium carbonate; In ethanol; 1,2-dichloro-ethane; acetone;
DOI:10.1021/jo302353g