TpOs(NHTol)Cl₂

Base Information

• Chemical Name: TpOs(NHTol)Cl₂
• CAS No.: 330945-66-9
• Molecular Formula: C₁₆H₁₈BCl₂N₇Os
• Molecular Weight: 580.283

Synonyms:TpOs(NHTol)Cl₂

Chemical Property of TpOs(NHTol)Cl₂

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Technology Process of TpOs(NHTol)Cl₂

There total 4 articles about TpOs(NHTol)Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

dichloro(hydrotris(1-pyrazolyl)borate)(nitrido)osmium(IV) + p-toluidine (106-49-0,12221-03-3) → TpOs(NHTol)Cl2 (330945-66-9)

Guidance literature:

With air; In dichloromethane; a bomb was charged with toluidine, Os-contg. compd. and CH2Cl2; the bombwas heated at 70°C for 1 d and then opened in the atmosphere; th en another portion of toluidine was added; heating at 70°C for 6 d; column chromy. (CH2Cl2 as eluant);

DOI:10.1021/ja0028424

Reference yield: 10.0%

dichloro(hydrotris(1-pyrazolyl)borate)(nitrido)osmium(IV) + triphenylborane (960-71-4) + tri-p-tolylborane (7297-94-1) + water (7732-18-5) → TpOs(NHPh)Cl2 + TpOs(NHTol)Cl2 (330945-66-9) + TpOs[N(Tol)(BPh2)]Cl2 + TpOs[N(Ph)(BTol2)]Cl2

Guidance literature:

In not given; a 10-fold excess of both BTol3 and BPh3; (1)H NMR studies;

DOI:10.1021/ja0028424

Reference yield:

dichloro(hydrotris(1-pyrazolyl)borate)(nitrido)osmium(IV) + tri-p-tolylborane (7297-94-1) + water (7732-18-5) → TpOs(NHTol)Cl2 (330945-66-9)

Guidance literature:

In not given; (1)H NMR studies;

DOI:10.1021/ja0028424

upstream raw materials:

BPh(Tol)2

tri-p-tolylborane

water

triphenylborane

Downstream raw materials:

[(hydrotris(1-pyrazolyl)borate)Os(anilino-d5)Cl₂]

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