threo-p-Methyldiphenylethandiol

Base Information

Chemical Name:threo-p-Methyldiphenylethandiol
CAS No.:62137-63-7
Molecular Formula:C₁₅H₁₆O₂
Molecular Weight:228.291
Hs Code.:

Synonyms:threo-p-Methyldiphenylethandiol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of threo-p-Methyldiphenylethandiol

Chemical Property:

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Technology Process of threo-p-Methyldiphenylethandiol

There total 10 articles about threo-p-Methyldiphenylethandiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2431-00-7
p-methylbenzil

: 62137-63-7
threo-p-Methyldiphenylethandiol

: 50600-29-8
C₁₅H₁₆O₂

Guidance literature:: With formic acid; triethylamine; In acetonitrile; at 50 ℃; for 40h; Overall yield = 92.5 %; enantioselective reaction;
DOI:10.1016/j.apcata.2014.03.039

Reference yield:

: 4714-21-0,130059-91-5,130059-95-9,1657-45-0,1860-17-9
E-1-methyl-4-styryl-benzene

: 62137-63-7
threo-p-Methyldiphenylethandiol

Guidance literature:: With 4-methylmorpholine N-oxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; potassium osmate(VI); sodium tetrachloropalladate(II); layered double-hydroxides(Mg-Al-Cl); In ethyl acetate; tert-butyl alcohol; at 20 ℃;

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 62137-63-7
threo-p-Methyldiphenylethandiol

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / Na₂PdCl₄/K₂OsO₄*2H₂O/layered double-hydroxides(Mg-Al-Cl) / 70 °C

2: Et₃N; (DHQD)2PHAL; N-methylmorpholine N-oxide / Na₂PdCl₄/K₂OsO₄*2H₂O/layered double-hydroxides(Mg-Al-Cl) / 2-methyl-propan-2-ol; ethyl acetate / 20 °C

With 4-methylmorpholine N-oxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; potassium osmate(VI); sodium tetrachloropalladate(II); layered double-hydroxides(Mg-Al-Cl); In ethyl acetate; tert-butyl alcohol; 1: Heck coupling;