hexahydro-3-phenyl-6,7,8-trihydroxy-3R-[3α,5β,6α,7β,8α,8aβ]-5H-oxazolo[3,2-α]pyridine-5-carbonitrile

Base Information

Chemical Name:hexahydro-3-phenyl-6,7,8-trihydroxy-3R-[3α,5β,6α,7β,8α,8aβ]-5H-oxazolo[3,2-α]pyridine-5-carbonitrile
CAS No.:307313-78-6
Molecular Formula:C₁₄H₁₆N₂O₄
Molecular Weight:276.292
Hs Code.:

Synonyms:hexahydro-3-phenyl-6,7,8-trihydroxy-3R-[3α,5β,6α,7β,8α,8aβ]-5H-oxazolo[3,2-α]pyridine-5-carbonitrile

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Chemical Property of hexahydro-3-phenyl-6,7,8-trihydroxy-3R-[3α,5β,6α,7β,8α,8aβ]-5H-oxazolo[3,2-α]pyridine-5-carbonitrile

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Technology Process of hexahydro-3-phenyl-6,7,8-trihydroxy-3R-[3α,5β,6α,7β,8α,8aβ]-5H-oxazolo[3,2-α]pyridine-5-carbonitrile

There total 2 articles about hexahydro-3-phenyl-6,7,8-trihydroxy-3R-[3α,5β,6α,7β,8α,8aβ]-5H-oxazolo[3,2-α]pyridine-5-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 19192-62-2,31459-16-2,57031-25-1,58117-04-7
xylo-pentodialdose

: 56613-80-0
D-2-phenylglycinol

: 151-50-8
potassium cyanide

: 307313-78-6
hexahydro-3-phenyl-6,7,8-trihydroxy-3R-[3α,5β,6α,7β,8α,8aβ]-5H-oxazolo[3,2-α]pyridine-5-carbonitrile

: 307313-77-5
hexahydro-3-phenyl-6,7,8-trihydroxy-3R-[3α,5β,6β,7α,8β,8aβ]-5H-oxazolo[3,2-α]pyridine-5-carbonitrile

Guidance literature:: xylo-pentodialdose; D-2-phenylglycinol; potassium cyanide; With citric buffer; In water;

With zinc dibromide; In methanol; for 3h; Further stages.;
DOI:10.1021/jo000434c

Reference yield: 15.0%

: 19192-62-2,31459-16-2,57031-25-1,58117-04-7
xylo-pentodialdose

: 56613-80-0
D-2-phenylglycinol

: 151-50-8
potassium cyanide

: (3R,5S,6R,7S,8R,8aS)-6,7,8-Trihydroxy-3-phenyl-hexahydro-oxazolo[3,2-a]pyridine-5-carbonitrile

: 307313-78-6
hexahydro-3-phenyl-6,7,8-trihydroxy-3R-[3α,5β,6α,7β,8α,8aβ]-5H-oxazolo[3,2-α]pyridine-5-carbonitrile

: 307313-77-5
hexahydro-3-phenyl-6,7,8-trihydroxy-3R-[3α,5β,6β,7α,8β,8aβ]-5H-oxazolo[3,2-α]pyridine-5-carbonitrile

Guidance literature:: xylo-pentodialdose; D-2-phenylglycinol; potassium cyanide; With citric acid; In water; at 20 ℃; for 15h;

With zinc dibromide; In methanol; for 4h;
DOI:10.1016/j.bmc.2004.07.039