Trifluoro-acetic acid (Z)-1-phenyl-5-trimethylsilanyl-pent-3-enyl ester

Base Information

Chemical Name:Trifluoro-acetic acid (Z)-1-phenyl-5-trimethylsilanyl-pent-3-enyl ester
CAS No.:873678-88-7
Molecular Formula:C₁₆H₂₁F₃O₂Si
Molecular Weight:330.422
Hs Code.:

Synonyms:Trifluoro-acetic acid (Z)-1-phenyl-5-trimethylsilanyl-pent-3-enyl ester

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Chemical Property of Trifluoro-acetic acid (Z)-1-phenyl-5-trimethylsilanyl-pent-3-enyl ester

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Technology Process of Trifluoro-acetic acid (Z)-1-phenyl-5-trimethylsilanyl-pent-3-enyl ester

There total 6 articles about Trifluoro-acetic acid (Z)-1-phenyl-5-trimethylsilanyl-pent-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133956-81-7
(Z)-1-phenyl-5-(trimethylsilyl)pent-3-en-1-ol

: 407-25-0
trifluoroacetic anhydride

: 873678-88-7
Trifluoro-acetic acid (Z)-1-phenyl-5-trimethylsilanyl-pent-3-enyl ester

Guidance literature:: With 2,6-dimethylpyridine; In diethyl ether;
DOI:10.1021/ja0536623

Reference yield:

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 873678-88-7
Trifluoro-acetic acid (Z)-1-phenyl-5-trimethylsilanyl-pent-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Grubbs second generation catalyst / CH₂Cl₂ / Heating

2: 2,6-lutidine / diethyl ether / -10 - 10 °C

With 2,6-dimethylpyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In diethyl ether; dichloromethane;
DOI:10.1021/jo062668n

Reference yield:

: 100-52-7
benzaldehyde

: 873678-88-7
Trifluoro-acetic acid (Z)-1-phenyl-5-trimethylsilanyl-pent-3-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Grubbs second generation catalyst / CH₂Cl₂ / Heating

2: 2,6-lutidine / diethyl ether / -10 - 10 °C

With 2,6-dimethylpyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In diethyl ether; dichloromethane;
DOI:10.1021/jo062668n