2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose

Base Information

Chemical Name:2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose
CAS No.:1447801-82-2
Molecular Formula:C₂₆H₃₅N₃O₆Si
Molecular Weight:513.666
Hs Code.:

Synonyms:2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose

Suppliers and Price of 2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 14 raw suppliers

Chemical Property of 2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose

Chemical Property:

Purity/Quality:: 98%Min ^*data from raw suppliers

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Technology Process of 2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose

There total 2 articles about 2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 613-90-1
benzoyl cyanide

: 120312-08-5
2-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose

: 1447801-82-2
2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose

Guidance literature:: With triethylamine; In acetonitrile; at -40 ℃; for 11h;
DOI:10.1021/jo400467g

Reference yield:

: 138889-14-2
2-azido-3-O-benzyl-4,6-O-benzylidene-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose

: 1447801-82-2
2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: ethanethiol; toluene-4-sulfonic acid / dichloromethane / 3 h / 20 °C

2: triethylamine / acetonitrile / 11 h / -40 °C

With toluene-4-sulfonic acid; triethylamine; ethanethiol; In dichloromethane; acetonitrile;
DOI:10.1021/jo400467g

Reference yield: 91.0%

: 1447801-82-2
2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-β-D-glucopyranose

: 123-76-2
levulinic acid

: 1447801-83-3
2-azido-6-O-benzoyl-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-2-deoxy-4-O-levulinoyl-β-D-glucopyranose

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/jo400467g