(S)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate

Base Information

Chemical Name:(S)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate
CAS No.:905991-76-6
Molecular Formula:C₁₆H₁₉NO₄S₂
Molecular Weight:353.463
Hs Code.:

Synonyms:(S)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate

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Chemical Property of (S)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate

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Technology Process of (S)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate

There total 3 articles about (S)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 308293-22-3
N-phenylmethylene 2-thiophenesulfonamide

: 89337-62-2
tert-butyl((1-methoxy-2-methylprop-1-en-1-yl)oxy)dimethylsilane

: 905991-76-6
(S)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate

: (R)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate

Guidance literature:: With silver perchlorate; chiral ferrocene-based phosphine copper; In dichloromethane; at 20 ℃; Title compound not separated from byproducts;
DOI:10.1021/ol060866v

Reference yield:

: 100-52-7
benzaldehyde

: 905991-76-6
(S)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / molecular sieves 4 Angstroem; Amberlyst-15 / toluene / 12 h / 120 °C

2: AgClO₄ / chiral ferrocene-based phosphine copper complex / CH₂Cl₂ / 20 °C

With amberlyst-15; 4 A molecular sieve; silver perchlorate; chiral ferrocene-based phosphine copper; In dichloromethane; toluene;
DOI:10.1021/ol060866v

Reference yield:

: 308293-22-3
N-phenylmethylene 2-thiophenesulfonamide

: 31469-15-5
1-methoxy-2-methyl-1-trimethylsiloxy-1-propene

: 905991-76-6
(S)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate

: (R)-methyl 2,2-dimethyl-3-phenyl-3-[(2-thienylsulfonyl)amino]propanoate

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); (S,S)-2,2'-isopropylidenebis(4-phenyl-2-oxazoline); In dichloromethane; at -78 ℃; for 24h; optical yield given as %ee;
DOI:10.1002/chem.200701425