1-Cyclohexylcarbonylaminoethyl-2-chloroacetyl-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:1-Cyclohexylcarbonylaminoethyl-2-chloroacetyl-1,2,3,4-tetrahydroisoquinoline
CAS No.:133958-43-7
Molecular Formula:C₂₀H₂₇ClN₂O₂
Molecular Weight:362.9
Hs Code.:

Synonyms:1-Cyclohexylcarbonylaminoethyl-2-chloroacetyl-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of 1-Cyclohexylcarbonylaminoethyl-2-chloroacetyl-1,2,3,4-tetrahydroisoquinoline

Chemical Property:

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Technology Process of 1-Cyclohexylcarbonylaminoethyl-2-chloroacetyl-1,2,3,4-tetrahydroisoquinoline

There total 3 articles about 1-Cyclohexylcarbonylaminoethyl-2-chloroacetyl-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 133958-42-6
1-Cyclohexylcarbonylaminoethyl-1,2,3,4-tetrahydroisoquinoline

: 79-04-9
chloroacetyl chloride

: 133958-43-7
1-Cyclohexylcarbonylaminoethyl-2-chloroacetyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With sodium hydroxide; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1007/BF00473968

Reference yield:

: (+/-)-1-(2-aminoethyl)-1,2,3,4-tetrahydroisoquinoline dihydrochloride

: 133958-43-7
1-Cyclohexylcarbonylaminoethyl-2-chloroacetyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / 2N NaOH, pyridine / acetonitrile / 3 h / 20 °C

2: 64 percent / 50percent NaOH / CH₂Cl₂ / 1 h / 20 °C

With pyridine; sodium hydroxide; In dichloromethane; acetonitrile;
DOI:10.1007/BF00473968

Reference yield:

: 2719-27-9
cyclohexanylcarbonyl chloride

: 133958-43-7
1-Cyclohexylcarbonylaminoethyl-2-chloroacetyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / 2N NaOH, pyridine / acetonitrile / 3 h / 20 °C

2: 64 percent / 50percent NaOH / CH₂Cl₂ / 1 h / 20 °C

With pyridine; sodium hydroxide; In dichloromethane; acetonitrile;
DOI:10.1007/BF00473968