2-(m-methoxyphenyl)cycloheptanol

Base Information

Chemical Name:2-(m-methoxyphenyl)cycloheptanol
CAS No.:75209-55-1
Molecular Formula:C₁₄H₂₀O₂
Molecular Weight:220.312
Hs Code.:

Synonyms:2-(m-methoxyphenyl)cycloheptanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(m-methoxyphenyl)cycloheptanol

Chemical Property:

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Technology Process of 2-(m-methoxyphenyl)cycloheptanol

There total 4 articles about 2-(m-methoxyphenyl)cycloheptanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2398-37-0
3-methoxyphenyl bromide

: 75209-55-1
2-(m-methoxyphenyl)cycloheptanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg / 1.) THF, 2.) THF, room temp., 30 min, 50-55 deg C, 1 h

2: oxalic acid / toluene / 16 h / Heating

3: 1.) NaBH₄, BF₃*Et₂O, 2.) 10percent NaOH, 30percent H₂O₂ / 1.) THF, room temp., 15 h, 2.) THF, H₂O, room temp., 1 h

With sodium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; oxalic acid; magnesium; In toluene;
DOI:10.1248/cpb.28.1022

Reference yield:

: 2082-28-2
1-(m-methoxyphenyl)cycloheptanol

: 75209-55-1
2-(m-methoxyphenyl)cycloheptanol

Guidance literature:: Multi-step reaction with 2 steps

1: oxalic acid / toluene / 16 h / Heating

2: 1.) NaBH₄, BF₃*Et₂O, 2.) 10percent NaOH, 30percent H₂O₂ / 1.) THF, room temp., 15 h, 2.) THF, H₂O, room temp., 1 h

With sodium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; oxalic acid; In toluene;
DOI:10.1248/cpb.28.1022

Reference yield:

: 502-42-1
cycloheptanone

: 75209-55-1
2-(m-methoxyphenyl)cycloheptanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg / 1.) THF, 2.) THF, room temp., 30 min, 50-55 deg C, 1 h

2: oxalic acid / toluene / 16 h / Heating

3: 1.) NaBH₄, BF₃*Et₂O, 2.) 10percent NaOH, 30percent H₂O₂ / 1.) THF, room temp., 15 h, 2.) THF, H₂O, room temp., 1 h

With sodium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; oxalic acid; magnesium; In toluene;
DOI:10.1248/cpb.28.1022