cis-1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-1-methyl-cyclohexyl]-propylamine

Base Information

Chemical Name:cis-1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-1-methyl-cyclohexyl]-propylamine
CAS No.:1202462-41-6
Molecular Formula:C₂₆H₃₁ClN₂O₂
Molecular Weight:438.997
Hs Code.:

Synonyms:cis-1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-1-methyl-cyclohexyl]-propylamine

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Chemical Property of cis-1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-1-methyl-cyclohexyl]-propylamine

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Technology Process of cis-1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-1-methyl-cyclohexyl]-propylamine

There total 5 articles about cis-1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-1-methyl-cyclohexyl]-propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 923022-55-3
1-benzyloxy-7-chloro-6-fluoro-isoquinoline

: 1202462-40-5
cis-4-(1-amino-propyl)-4-methyl-cyclohexanol

: 1202462-41-6
cis-1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-1-methyl-cyclohexyl]-propylamine

Guidance literature:: cis-4-(1-amino-propyl)-4-methyl-cyclohexanol; With sodium hydride; In ISOPROPYLAMIDE; for 0.166667h;

1-benzyloxy-7-chloro-6-fluoro-isoquinoline; In ISOPROPYLAMIDE; at 50 ℃; for 3h; Inert atmosphere;

Reference yield:

: C₁₀H₁₉NO

: 1202462-41-6
cis-1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-1-methyl-cyclohexyl]-propylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / ethanol / 4 h / Reflux

2.1: sodium hydride / ISOPROPYLAMIDE / 0.17 h

2.2: 3 h / 50 °C / Inert atmosphere

With sodium tetrahydroborate; sodium hydride; In ethanol; ISOPROPYLAMIDE;

Reference yield:

: 121955-82-6
1-methyl-4-oxocyclohexane-1-carbonitrile

: 1202462-41-6
cis-1-[4-(1-benzyloxy-7-chloro-isoquinolin-6-yloxy)-1-methyl-cyclohexyl]-propylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / ethanol / -65 °C

2.1: diethyl ether / 4 h / Reflux

3.1: sodium tetrahydroborate / ethanol / 4 h / Reflux

4.1: sodium hydride / ISOPROPYLAMIDE / 0.17 h

4.2: 3 h / 50 °C / Inert atmosphere

With sodium tetrahydroborate; sodium hydride; In diethyl ether; ethanol; ISOPROPYLAMIDE;