(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-amine

Base Information

Chemical Name:(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-amine
CAS No.:945723-55-7
Molecular Formula:C₂₄H₃₂N₄O₄S₂
Molecular Weight:504.674
Hs Code.:

Synonyms:(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-amine

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Technology Process of (2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-amine

There total 7 articles about (2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 945723-54-6
(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-azide

: 945723-55-7
(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-amine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 24h;
DOI:10.1002/chem.200601420

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 945723-55-7
(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / triethylamine / CHCl₃ / 12 h / 20 °C

2: 63 percent / NaBH₄ / methanol / 2 h / 0 °C

3: 94 percent / triethylamine; AcOEt / 1.5 h / 0 - 20 °C

4: 93 percent / NaN₃ / dimethylformamide / 5 h / 20 °C

5: 71 percent / hydrogen / Pd/C / methanol / 24 h / 20 °C

With sodium tetrahydroborate; sodium azide; hydrogen; ethyl acetate; triethylamine; palladium on activated charcoal; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601420

Reference yield:

: 4467-54-3,5619-10-3,7389-87-9,18684-16-7,22888-60-4,32381-17-2,92742-29-5,100009-20-9
l-histidine methyl ester dihydrochloride

: 945723-55-7
(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / triethylamine / CHCl₃ / 12 h / 20 °C

2: 63 percent / NaBH₄ / methanol / 2 h / 0 °C

3: 94 percent / triethylamine; AcOEt / 1.5 h / 0 - 20 °C

4: 93 percent / NaN₃ / dimethylformamide / 5 h / 20 °C

5: 71 percent / hydrogen / Pd/C / methanol / 24 h / 20 °C

With sodium tetrahydroborate; sodium azide; hydrogen; ethyl acetate; triethylamine; palladium on activated charcoal; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601420