(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-azide

Base Information

Chemical Name:(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-azide
CAS No.:945723-54-6
Molecular Formula:C₂₄H₃₀N₆O₄S₂
Molecular Weight:530.672
Hs Code.:

Synonyms:(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-azide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-azide

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Technology Process of (2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-azide

There total 5 articles about (2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 945723-54-6
(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-azide

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / triethylamine / CHCl₃ / 12 h / 20 °C

2: 63 percent / NaBH₄ / methanol / 2 h / 0 °C

3: 94 percent / triethylamine; AcOEt / 1.5 h / 0 - 20 °C

4: 93 percent / NaN₃ / dimethylformamide / 5 h / 20 °C

With sodium tetrahydroborate; sodium azide; ethyl acetate; triethylamine; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601420

Reference yield:

: 4467-54-3,5619-10-3,7389-87-9,18684-16-7,22888-60-4,32381-17-2,92742-29-5,100009-20-9
l-histidine methyl ester dihydrochloride

: 945723-54-6
(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-azide

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / triethylamine / CHCl₃ / 12 h / 20 °C

2: 63 percent / NaBH₄ / methanol / 2 h / 0 °C

3: 94 percent / triethylamine; AcOEt / 1.5 h / 0 - 20 °C

4: 93 percent / NaN₃ / dimethylformamide / 5 h / 20 °C

With sodium tetrahydroborate; sodium azide; ethyl acetate; triethylamine; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601420

Reference yield:

: 71-00-1,26062-48-6,90081-11-1
L-histidine

: 945723-54-6
(2S)-2-(2,4,6-trimethylbenzenesulfonamido)-3-[1-(2,4,6-trimethylbenzenesulfonyl)imidazol-4-yl]prop-1-yl-azide

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / AcCl / 24 h

2: 90 percent / triethylamine / CHCl₃ / 12 h / 20 °C

3: 63 percent / NaBH₄ / methanol / 2 h / 0 °C

4: 94 percent / triethylamine; AcOEt / 1.5 h / 0 - 20 °C

5: 93 percent / NaN₃ / dimethylformamide / 5 h / 20 °C

With sodium tetrahydroborate; sodium azide; ethyl acetate; triethylamine; acetyl chloride; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601420