7,8-Dimethoxy-6-methyl-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepine-3-carbaldehyde

Base Information

Chemical Name:7,8-Dimethoxy-6-methyl-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepine-3-carbaldehyde
CAS No.:78495-79-1
Molecular Formula:C₂₀H₂₃NO₃
Molecular Weight:325.408
Hs Code.:

Synonyms:7,8-Dimethoxy-6-methyl-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepine-3-carbaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7,8-Dimethoxy-6-methyl-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepine-3-carbaldehyde

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Technology Process of 7,8-Dimethoxy-6-methyl-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepine-3-carbaldehyde

There total 1 articles about 7,8-Dimethoxy-6-methyl-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepine-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 71157-99-8
6-methyl-7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine hydrochloride

: 109-94-4
formic acid ethyl ester

: 78495-79-1
7,8-Dimethoxy-6-methyl-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepine-3-carbaldehyde

Guidance literature:: at 25 ℃; for 24h;
DOI:10.1021/jm00161a029

Reference yield:

: 78495-79-1
7,8-Dimethoxy-6-methyl-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepine-3-carbaldehyde

: 104113-79-3
7,8-dimethoxy-3,6-dimethyl-1-phenyl-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Guidance literature:: With borane; In tetrahydrofuran; at 25 ℃; for 16h;
DOI:10.1021/jm00161a029

Reference yield:

: 78495-79-1
7,8-Dimethoxy-6-methyl-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepine-3-carbaldehyde

: 71157-98-7
3,6-dimethyl-7,8-dihydroxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: BH₃ / tetrahydrofuran / 16 h / 25 °C

2: 37 percent / BBr₃ / 3.5 h

With borane; boron tribromide; In tetrahydrofuran;
DOI:10.1021/jm00161a029