2-(R)-[18O]hydroxy-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane

Base Information

• Chemical Name: 2-(R)-[18O]hydroxy-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane
• CAS No.: 344913-70-8
• Molecular Formula: C₁₁H₁₅O₄P
• Molecular Weight: 244.212

Synonyms:2-(R)-[18O]hydroxy-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane

Chemical Property of 2-(R)-[18O]hydroxy-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane

Chemical Property:

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Technology Process of 2-(R)-[18O]hydroxy-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane

There total 1 articles about 2-(R)-[18O]hydroxy-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(-)-(R)-2-chloro-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane (148616-42-6) → 2-(R)-[18O]hydroxy-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane (344913-70-8)

Guidance literature:

With potassium tert-butylate; ¹⁸O-labeled water; tert-butyl alcohol; for 1h;

DOI:10.1021/ja004084n

Reference yield:

(-)-(R)-2-chloro-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane (148616-42-6) + 2-(R)-[18O]hydroxy-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane (344913-70-8) → C22H28O6(18)OP2 + C22H28O6(18)OP2

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1021/ja004084n

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2-(R)-[18O]hydroxy-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane (344913-70-8) → C12H17O3(18)OP + C12H17O3(18)OP

Guidance literature:

Title compound not separated from byproducts.;

DOI:10.1021/ja004084n

upstream raw materials:

(-)-(R)-2-chloro-2-oxo-5,5-dimethyl-4-(R)-phenyl-1,3,2-dioxaphosphorinane

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