3-benzyl-6,6-dimethyl-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

Base Information

Chemical Name:3-benzyl-6,6-dimethyl-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione
CAS No.:1363495-03-7
Molecular Formula:C₁₆H₁₈N₂O₂
Molecular Weight:270.331
Hs Code.:

Synonyms:3-benzyl-6,6-dimethyl-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

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Chemical Property of 3-benzyl-6,6-dimethyl-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

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Technology Process of 3-benzyl-6,6-dimethyl-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

There total 4 articles about 3-benzyl-6,6-dimethyl-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1363495-01-5
1,3-dibenzyl-6,6-dimethyl-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

: 1363495-03-7
3-benzyl-6,6-dimethyl-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

Guidance literature:: With palladium 10% on activated carbon; ammonium formate; In methanol; for 15h; regioselective reaction; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.01.060

Reference yield:

: 1807-68-7
diazodimedone

: 1363495-03-7
3-benzyl-6,6-dimethyl-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 5 h / 110 °C / Inert atmosphere

2: potassium carbonate / toluene / 10 h / 110 °C / Inert atmosphere

3: palladium 10% on activated carbon; ammonium formate / methanol / 15 h / Inert atmosphere; Reflux

With palladium 10% on activated carbon; ammonium formate; potassium carbonate; In methanol; toluene;
DOI:10.1016/j.tet.2012.01.060

Reference yield:

: 126-81-8
dimedone

: 1363495-03-7
3-benzyl-6,6-dimethyl-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

Guidance literature:: Multi-step reaction with 4 steps

1: aryl azide / Inert atmosphere

2: toluene / 5 h / 110 °C / Inert atmosphere

3: potassium carbonate / toluene / 10 h / 110 °C / Inert atmosphere

4: palladium 10% on activated carbon; ammonium formate / methanol / 15 h / Inert atmosphere; Reflux

With palladium 10% on activated carbon; ammonium formate; potassium carbonate; In methanol; toluene;
DOI:10.1016/j.tet.2012.01.060