3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-N-octadecyl-β-D-mannopyranosylamine

Base Information

Chemical Name:3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-N-octadecyl-β-D-mannopyranosylamine
CAS No.:157609-17-1
Molecular Formula:C₅₁H₈₃NO₅
Molecular Weight:790.224
Hs Code.:

Synonyms:3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-N-octadecyl-β-D-mannopyranosylamine

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Chemical Property of 3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-N-octadecyl-β-D-mannopyranosylamine

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Technology Process of 3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-N-octadecyl-β-D-mannopyranosylamine

There total 4 articles about 3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-N-octadecyl-β-D-mannopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 157609-16-0
N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-β-D-glucopyranosyl)-N-(octadecyl)dodecanamide

: 157609-17-1
3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-N-octadecyl-β-D-mannopyranosylamine

Guidance literature:: With pyridine; methanesulfonyl chloride; for 8h; Ambient temperature;

Reference yield:

: 142864-32-2
(1S,2R,3R,5R,8R,10S)-2-benzyloxy-5-phenyl-4,6,11-trioxatricyclo<8.1.0^3.8>undecane

: 157609-17-1
3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-N-octadecyl-β-D-mannopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 25 percent / propan-2-ol / 96 h / 120 °C

2: 55 percent / diethyl cyanophosphonate, Et₃N / dimethylformamide / 3 h / 0 °C

3: 61 percent / pyridine, mesyl chloride / 8 h / Ambient temperature

With pyridine; diethyl cyanophosphonate; methanesulfonyl chloride; triethylamine; In N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 124-30-1
1-aminooctadecane

: 157609-17-1
3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-N-octadecyl-β-D-mannopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 25 percent / propan-2-ol / 96 h / 120 °C

2: 55 percent / diethyl cyanophosphonate, Et₃N / dimethylformamide / 3 h / 0 °C

3: 61 percent / pyridine, mesyl chloride / 8 h / Ambient temperature

With pyridine; diethyl cyanophosphonate; methanesulfonyl chloride; triethylamine; In N,N-dimethyl-formamide; isopropyl alcohol;