N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-β-D-mannopyranosyl)-N-(octadecyl)dodecanamide

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Chemical Name:N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-β-D-mannopyranosyl)-N-(octadecyl)dodecanamide
CAS No.:157609-18-2
Molecular Formula:C₆₃H₁₀₅NO₆
Molecular Weight:972.53
Hs Code.:

Synonyms:N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-β-D-mannopyranosyl)-N-(octadecyl)dodecanamide

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Chemical Property of N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-β-D-mannopyranosyl)-N-(octadecyl)dodecanamide

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Technology Process of N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-β-D-mannopyranosyl)-N-(octadecyl)dodecanamide

There total 5 articles about N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-β-D-mannopyranosyl)-N-(octadecyl)dodecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 112-16-3
n-dodecanoyl chloride

: 157609-17-1
3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-N-octadecyl-β-D-mannopyranosylamine

: 157609-18-2
N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-β-D-mannopyranosyl)-N-(octadecyl)dodecanamide

Guidance literature:: With dmap; In dichloromethane; at 0 ℃; for 3h;

Reference yield:

: 142864-32-2
(1S,2R,3R,5R,8R,10S)-2-benzyloxy-5-phenyl-4,6,11-trioxatricyclo<8.1.0^3.8>undecane

: 157609-18-2
N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-β-D-mannopyranosyl)-N-(octadecyl)dodecanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 25 percent / propan-2-ol / 96 h / 120 °C

2: 55 percent / diethyl cyanophosphonate, Et₃N / dimethylformamide / 3 h / 0 °C

3: 61 percent / pyridine, mesyl chloride / 8 h / Ambient temperature

4: 90 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 3 h / 0 °C

With pyridine; dmap; diethyl cyanophosphonate; methanesulfonyl chloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 124-30-1
1-aminooctadecane

: 157609-18-2
N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-β-D-mannopyranosyl)-N-(octadecyl)dodecanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 25 percent / propan-2-ol / 96 h / 120 °C

2: 55 percent / diethyl cyanophosphonate, Et₃N / dimethylformamide / 3 h / 0 °C

3: 61 percent / pyridine, mesyl chloride / 8 h / Ambient temperature

4: 90 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 3 h / 0 °C

With pyridine; dmap; diethyl cyanophosphonate; methanesulfonyl chloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;