C₄₂H₅₄N₄O₄

Base Information

Chemical Name:C₄₂H₅₄N₄O₄
CAS No.:1430817-34-7
Molecular Formula:C₄₂H₅₄N₄O₄
Molecular Weight:678.915
Hs Code.:

C<sub>42</sub>H<sub>54</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:C₄₂H₅₄N₄O₄

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Chemical Property of C₄₂H₅₄N₄O₄

Chemical Property:

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Technology Process of C₄₂H₅₄N₄O₄

There total 11 articles about C₄₂H₅₄N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1430817-33-6
C₅₂H₇₀N₄O₈

: 1430817-34-7
C₄₂H₅₄N₄O₄

Guidance literature:: With dimethylsulfide; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1016/j.cclet.2013.02.014

Reference yield:

: 59-92-7,90638-38-3
levodopa

: 1430817-34-7
C₄₂H₅₄N₄O₄

Guidance literature:: Multi-step reaction with 10 steps

1: thionyl chloride / 72 h / 20 °C

2: sodium acetate; acetic acid / 20 h / 20 °C

3: sodium formate; acetic anhydride / 4 h / 20 °C

4: potassium carbonate / acetone / 10 h / Reflux

5: hydrogenchloride / methanol / 3 h / Reflux

6: triethylamine / dichloromethane / 16 h / 20 °C

7: diisobutylaluminium hydride / toluene / 1.5 h / -78 °C

8: methanol / 0.5 h / 20 °C

9: sodium cyanoborohydride / methanol / 5 h / 20 °C

10: trifluoroacetic acid; dimethylsulfide / dichloromethane / 0.5 h / 20 °C

With hydrogenchloride; thionyl chloride; dimethylsulfide; sodium formate; sodium acetate; acetic anhydride; diisobutylaluminium hydride; sodium cyanoborohydride; potassium carbonate; acetic acid; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; acetone; toluene; 2: |Pictet-Spengler Synthesis;
DOI:10.1016/j.cclet.2013.02.014

Reference yield:

: 1173933-70-4
C₁₇H₁₇NO₄

: 1430817-34-7
C₄₂H₅₄N₄O₄

Guidance literature:: Multi-step reaction with 8 steps

1: sodium formate; acetic anhydride / 4 h / 20 °C

2: potassium carbonate / acetone / 10 h / Reflux

3: hydrogenchloride / methanol / 3 h / Reflux

4: triethylamine / dichloromethane / 16 h / 20 °C

5: diisobutylaluminium hydride / toluene / 1.5 h / -78 °C

6: methanol / 0.5 h / 20 °C

7: sodium cyanoborohydride / methanol / 5 h / 20 °C

8: trifluoroacetic acid; dimethylsulfide / dichloromethane / 0.5 h / 20 °C

With hydrogenchloride; dimethylsulfide; sodium formate; acetic anhydride; diisobutylaluminium hydride; sodium cyanoborohydride; potassium carbonate; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; acetone; toluene;
DOI:10.1016/j.cclet.2013.02.014