methoxy>trimethylsilane

Base Information

Chemical Name:methoxy>trimethylsilane
CAS No.:153617-80-2
Molecular Formula:C₂₅H₃₀O₃Si
Molecular Weight:406.597
Hs Code.:

<cyclopentylidene<3,6-dimethoxy-2-(phenylethynyl)phenyl>methoxy>trimethylsilane

Synonyms:methoxy>trimethylsilane

Suppliers and Price of methoxy>trimethylsilane

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Chemical Property of methoxy>trimethylsilane

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Technology Process of methoxy>trimethylsilane

There total 4 articles about methoxy>trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 153617-79-9
<3,6-dimethoxy-2-(phenylethynyl)phenyl>methanone

: 153617-80-2
methoxy>trimethylsilane

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/S0040-4020(01)88016-9

Reference yield:

: 872-53-7
cyclopentanealdehyde

: 153617-80-2
methoxy>trimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-BuLi / 1) hexane, ether, -78 deg C, 30 min, 2) hexane, ether, -78 to 0 deg C, 2 h

2: 85 percent / pyridinium chlorochromate, 3A mol. sieves / CH₂Cl₂ / 6 h / Ambient temperature

3: 92 percent / Et₃N / CH₂Cl₂ / 1 h / 0 °C

With n-butyllithium; 3 A molecular sieve; triethylamine; pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/S0040-4020(01)88016-9

Reference yield:

: 107135-56-8
2-bromo-1,4-dimethoxy-3-(phenylethynyl)benzene

: 153617-80-2
methoxy>trimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-BuLi / 1) hexane, ether, -78 deg C, 30 min, 2) hexane, ether, -78 to 0 deg C, 2 h

2: 85 percent / pyridinium chlorochromate, 3A mol. sieves / CH₂Cl₂ / 6 h / Ambient temperature

3: 92 percent / Et₃N / CH₂Cl₂ / 1 h / 0 °C

With n-butyllithium; 3 A molecular sieve; triethylamine; pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/S0040-4020(01)88016-9