4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoic acid

Base Information

Chemical Name:4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoic acid
CAS No.:1621680-68-9
Molecular Formula:C₂₃H₂₀ClNO₄
Molecular Weight:409.869
Hs Code.:

Synonyms:4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoic acid

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Chemical Property of 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoic acid

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Technology Process of 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoic acid

There total 8 articles about 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1621681-50-2
ethyl 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoate

: 1621680-68-9
4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoic acid

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; at 80 ℃;

Reference yield:

: 3095-50-9
3,5-dimethyl-4-nitrobenzoic acid ethyl ester

: 1621680-68-9
4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate; ethanol / 20 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

3: palladium diacetate; sodium carbonate / methanol; water / 0.5 h / 140 °C / Inert atmosphere; Microwave irradiation

4: sodium hydroxide; water / tetrahydrofuran / 80 °C

With palladium 10% on activated carbon; water; hydrogen; palladium diacetate; sodium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 3095-47-4
4-amino-3,5-dimethylbenzoic acid ethyl ester

: 1621680-68-9
4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

2: palladium diacetate; sodium carbonate / methanol; water / 0.5 h / 140 °C / Inert atmosphere; Microwave irradiation

3: sodium hydroxide; water / tetrahydrofuran / 80 °C

With water; palladium diacetate; sodium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;