ethyl 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoate

Base Information

Chemical Name:ethyl 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoate
CAS No.:1621681-50-2
Molecular Formula:C₂₅H₂₄ClNO₄
Molecular Weight:437.923
Hs Code.:

Synonyms:ethyl 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoate

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Chemical Property of ethyl 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoate

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Technology Process of ethyl 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoate

There total 6 articles about ethyl 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1621681-39-7
ethyl 4-(5-bromo-2-chlorobenzamido)-3,5-dimethylbenzoate

: 10365-98-7,1107579-37-2
3-methoxyphenylboronic acid

: 1621681-50-2
ethyl 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoate

Guidance literature:: With palladium diacetate; sodium carbonate; In methanol; water; at 140 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 3095-47-4
4-amino-3,5-dimethylbenzoic acid ethyl ester

: 1621681-50-2
ethyl 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

2: palladium diacetate; sodium carbonate / methanol; water / 0.5 h / 140 °C / Inert atmosphere; Microwave irradiation

With palladium diacetate; sodium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 21739-92-4
5-bromo-2-chlorobenzoic acid

: 1621681-50-2
ethyl 4-(4-chloro-3'-methoxybiphenyl-3-ylcarboxamido)-3,5-dimethylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

3: palladium diacetate; sodium carbonate / methanol; water / 0.5 h / 140 °C / Inert atmosphere; Microwave irradiation

With oxalyl dichloride; palladium diacetate; sodium carbonate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;