Technology Process of {Cu2(C32H40N6)(CO)2}(2+)*2PF6(1-)={Cu2(C32H40N6)(CO)2}(PF6)2
There total 1 articles about {Cu2(C32H40N6)(CO)2}(2+)*2PF6(1-)={Cu2(C32H40N6)(CO)2}(PF6)2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
CO;
In
methanol;
C32H40N6 dissolved in CO-saturated methanol and dropped to solid {Cu(CH3CN)4}{PF6} under Ar;; formed ppt. allowed to stir for 2h with added diethyl ether; obtained {Cu2(C32H40N6)(CO)2}(PF6)2 recrystd. from CH2Cl2/(C2H5)2O; elem.analysis;
DOI:10.1021/ja00212a031