3-((3-(6-nitrobenzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl)methyl)-2-(4-nitrophenyl)-1,3,4-thiadiazol-3-ium-5-thiolate

Base Information

Chemical Name:3-((3-(6-nitrobenzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl)methyl)-2-(4-nitrophenyl)-1,3,4-thiadiazol-3-ium-5-thiolate
CAS No.:1612240-70-6
Molecular Formula:C₂₄H₁₃N₇O₅S₃
Molecular Weight:575.609
Hs Code.:

Synonyms:3-((3-(6-nitrobenzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl)methyl)-2-(4-nitrophenyl)-1,3,4-thiadiazol-3-ium-5-thiolate

Suppliers and Price of 3-((3-(6-nitrobenzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl)methyl)-2-(4-nitrophenyl)-1,3,4-thiadiazol-3-ium-5-thiolate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-((3-(6-nitrobenzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl)methyl)-2-(4-nitrophenyl)-1,3,4-thiadiazol-3-ium-5-thiolate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-((3-(6-nitrobenzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl)methyl)-2-(4-nitrophenyl)-1,3,4-thiadiazol-3-ium-5-thiolate

There total 4 articles about 3-((3-(6-nitrobenzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl)methyl)-2-(4-nitrophenyl)-1,3,4-thiadiazol-3-ium-5-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1612240-65-9
potassium 2-{[3-(6-nitro-1,3-benzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl]methyl}hydrazine carbodithioate

: 122-04-3
4-nitro-benzoyl chloride

: 1612240-70-6
3-((3-(6-nitrobenzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl)methyl)-2-(4-nitrophenyl)-1,3,4-thiadiazol-3-ium-5-thiolate

Guidance literature:: In water; at 20 ℃; for 2h;
DOI:10.1080/10426507.2013.829839

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 1612240-70-6
3-((3-(6-nitrobenzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl)methyl)-2-(4-nitrophenyl)-1,3,4-thiadiazol-3-ium-5-thiolate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / benzene / 5 h / Reflux

2: potassium carbonate / benzene / 2 h / Reflux

3: hydrazine hydrate / ethanol / 10 h / Reflux

4: potassium hydroxide / ethanol / 1 h / 20 °C

5: water / 2 h / 20 °C

With pyridine; potassium carbonate; hydrazine hydrate; potassium hydroxide; In ethanol; water; benzene;
DOI:10.1080/10426507.2013.829839

Reference yield:

: 14422-49-2
2-chloroacetamidobenzoic acid

: 1612240-70-6
3-((3-(6-nitrobenzo[d]thiazol-2-yl)-4-oxo-3,4-dihydroquinazolin-2-yl)methyl)-2-(4-nitrophenyl)-1,3,4-thiadiazol-3-ium-5-thiolate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / benzene / 2 h / Reflux

2: hydrazine hydrate / ethanol / 10 h / Reflux

3: potassium hydroxide / ethanol / 1 h / 20 °C

4: water / 2 h / 20 °C

With potassium carbonate; hydrazine hydrate; potassium hydroxide; In ethanol; water; benzene;
DOI:10.1080/10426507.2013.829839