2,3-di[benzyl(11-tetrahydropyranyloxy-3,6,9-trioxoundecyl)amino]-2-butene-1,4-dinitrile

Base Information

Chemical Name:2,3-di[benzyl(11-tetrahydropyranyloxy-3,6,9-trioxoundecyl)amino]-2-butene-1,4-dinitrile
CAS No.:674780-14-4
Molecular Formula:C₄₄H₆₄N₄O₁₀
Molecular Weight:809.013
Hs Code.:

Synonyms:2,3-di[benzyl(11-tetrahydropyranyloxy-3,6,9-trioxoundecyl)amino]-2-butene-1,4-dinitrile

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Chemical Property of 2,3-di[benzyl(11-tetrahydropyranyloxy-3,6,9-trioxoundecyl)amino]-2-butene-1,4-dinitrile

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Technology Process of 2,3-di[benzyl(11-tetrahydropyranyloxy-3,6,9-trioxoundecyl)amino]-2-butene-1,4-dinitrile

There total 2 articles about 2,3-di[benzyl(11-tetrahydropyranyloxy-3,6,9-trioxoundecyl)amino]-2-butene-1,4-dinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: (Z)-2,3-Bis-benzylamino-but-2-enedinitrile

: 674780-12-2
11-iodo-1-tetrahydropyranyloxy-3,6,9-trioxaundecane

: 674780-14-4
2,3-di[benzyl(11-tetrahydropyranyloxy-3,6,9-trioxoundecyl)amino]-2-butene-1,4-dinitrile

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; for 19h;
DOI:10.1016/j.tet.2003.09.060

Reference yield:

: 128660-97-9
2-(2-(2-(2-((tetrahydro-2H-pyran-2-yl)oxy)ethoxy)ethoxy)ethoxy)ethan-1-ol

: 674780-14-4
2,3-di[benzyl(11-tetrahydropyranyloxy-3,6,9-trioxoundecyl)amino]-2-butene-1,4-dinitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / I₂; PPh₃; imidazole / acetonitrile; diethyl ether / 2 h / cooling

2: 87 percent / Cs₂CO₃ / dimethylformamide / 19 h

With 1H-imidazole; iodine; caesium carbonate; triphenylphosphine; In diethyl ether; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2003.09.060