4-(1,3-dimethyl-1H-pyrazolo[4,3-e][1,2,4]triazin-5-ylamino)benzene-1-sulfonyl chloride

Base Information

Chemical Name:4-(1,3-dimethyl-1H-pyrazolo[4,3-e][1,2,4]triazin-5-ylamino)benzene-1-sulfonyl chloride
CAS No.:1606992-07-7
Molecular Formula:C₁₂H₁₁ClN₆O₂S
Molecular Weight:338.777
Hs Code.:

Synonyms:4-(1,3-dimethyl-1H-pyrazolo[4,3-e][1,2,4]triazin-5-ylamino)benzene-1-sulfonyl chloride

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Chemical Property of 4-(1,3-dimethyl-1H-pyrazolo[4,3-e][1,2,4]triazin-5-ylamino)benzene-1-sulfonyl chloride

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Technology Process of 4-(1,3-dimethyl-1H-pyrazolo[4,3-e][1,2,4]triazin-5-ylamino)benzene-1-sulfonyl chloride

There total 4 articles about 4-(1,3-dimethyl-1H-pyrazolo[4,3-e][1,2,4]triazin-5-ylamino)benzene-1-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1606992-08-8
1,3-dimethyl-5-phenylamino-1H-pyrazolo[4,3-e][1,2,4]triazine

: 1606992-07-7
4-(1,3-dimethyl-1H-pyrazolo[4,3-e][1,2,4]triazin-5-ylamino)benzene-1-sulfonyl chloride

Guidance literature:: With chlorosulfonic acid; at 20 ℃; for 2h; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.ejmech.2014.03.054

Reference yield:

: 682319-80-8
1,3-dimethyl-5-(methylsulfanyl)-1H-pyrazolo[4,3-e][1,2,4]triazine

: 1606992-07-7
4-(1,3-dimethyl-1H-pyrazolo[4,3-e][1,2,4]triazin-5-ylamino)benzene-1-sulfonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium permanganate; tetrabutylammomium bromide / acetic acid; benzene; water / 2 h / 20 °C

2: 216 h / 150 °C / Sealed tube

3: chlorosulfonic acid / 2 h / 20 °C / Inert atmosphere; Cooling with ice

With chlorosulfonic acid; potassium permanganate; tetrabutylammomium bromide; In water; acetic acid; benzene;
DOI:10.1016/j.ejmech.2014.03.054

Reference yield:

: 960307-19-1
C₇H₁₁N₅S

: 1606992-07-7
4-(1,3-dimethyl-1H-pyrazolo[4,3-e][1,2,4]triazin-5-ylamino)benzene-1-sulfonyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid

2: potassium permanganate; tetrabutylammomium bromide / acetic acid; benzene; water / 2 h / 20 °C

3: 216 h / 150 °C / Sealed tube

4: chlorosulfonic acid / 2 h / 20 °C / Inert atmosphere; Cooling with ice

With chlorosulfonic acid; potassium permanganate; tetrabutylammomium bromide; toluene-4-sulfonic acid; In water; acetic acid; benzene;
DOI:10.1016/j.ejmech.2014.03.054