3,5-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;5,4-d']diisoxazole 4,4-dioxide

Base Information

Chemical Name:3,5-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;5,4-d']diisoxazole 4,4-dioxide
CAS No.:86597-90-2
Molecular Formula:C₁₈H₁₄N₂O₄S
Molecular Weight:354.386
Hs Code.:

Synonyms:3,5-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;5,4-d']diisoxazole 4,4-dioxide

Suppliers and Price of 3,5-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;5,4-d']diisoxazole 4,4-dioxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;5,4-d']diisoxazole 4,4-dioxide

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Technology Process of 3,5-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;5,4-d']diisoxazole 4,4-dioxide

There total 11 articles about 3,5-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;5,4-d']diisoxazole 4,4-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 15091-30-2
3,4-dibromo-2,3,4,5-tetrahydrothiophene-1,1-dioxide

: 934-16-7
phenylhydroxamoyl chloride

: 86597-89-9
3-Phenyl-3a,6a-dihydro-thieno[2,3-d]isoxazole 4,4-dioxide

: 86597-90-2
3,5-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;5,4-d']diisoxazole 4,4-dioxide

Guidance literature:: With triethylamine; In benzene; for 48h; Ambient temperature;
DOI:10.1016/0040-4020(82)80071-9

Reference yield: 0.8%

: 873-67-6
benzonitrile oxide

: 86597-89-9
3-Phenyl-3a,6a-dihydro-thieno[2,3-d]isoxazole 4,4-dioxide

: 86612-75-1
3,7-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;4,5-d']diisoxazole 4,4-dioxide

: 86597-90-2
3,5-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;5,4-d']diisoxazole 4,4-dioxide

Guidance literature:: With triethylamine; In benzene; Yield given; Ambient temperature;
DOI:10.1016/0040-4020(82)80071-9

Reference yield:

: 873-67-6
benzonitrile oxide

: 86597-90-2
3,5-Diphenyl-3a,4a,7a,7b-tetrahydro-thieno[2,3-d;5,4-d']diisoxazole 4,4-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / benzene / 0.08 h

2: Et₃N / benzene / Ambient temperature

With triethylamine; In benzene;
DOI:10.1016/0040-4020(82)80071-9