1-benzyl 3a-ethyl 4-oxo-3,3a,4,5-tetrahydro-1H-pyrrolo[3,2-c]quinoline-1,3a(2H,9bH)-dicarboxylate

Base Information

Chemical Name:1-benzyl 3a-ethyl 4-oxo-3,3a,4,5-tetrahydro-1H-pyrrolo[3,2-c]quinoline-1,3a(2H,9bH)-dicarboxylate
CAS No.:1426301-91-8
Molecular Formula:C₂₂H₂₂N₂O₅
Molecular Weight:394.427
Hs Code.:

Synonyms:1-benzyl 3a-ethyl 4-oxo-3,3a,4,5-tetrahydro-1H-pyrrolo[3,2-c]quinoline-1,3a(2H,9bH)-dicarboxylate

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Chemical Property of 1-benzyl 3a-ethyl 4-oxo-3,3a,4,5-tetrahydro-1H-pyrrolo[3,2-c]quinoline-1,3a(2H,9bH)-dicarboxylate

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Technology Process of 1-benzyl 3a-ethyl 4-oxo-3,3a,4,5-tetrahydro-1H-pyrrolo[3,2-c]quinoline-1,3a(2H,9bH)-dicarboxylate

There total 3 articles about 1-benzyl 3a-ethyl 4-oxo-3,3a,4,5-tetrahydro-1H-pyrrolo[3,2-c]quinoline-1,3a(2H,9bH)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1426301-90-7
1-benzyl 3,3-diethyl 2-(2-nitrophenyl)pyrrolidine-1,3,3-tricarboxylate

: 1426301-91-8
1-benzyl 3a-ethyl 4-oxo-3,3a,4,5-tetrahydro-1H-pyrrolo[3,2-c]quinoline-1,3a(2H,9bH)-dicarboxylate

Guidance literature:: With iron; acetic acid; at 80 ℃; for 5h;
DOI:10.1039/c3ob27472a

Reference yield:

: 53844-02-3
benzyl N-(2-bromoethyl)carbamate

: 1426301-91-8
1-benzyl 3a-ethyl 4-oxo-3,3a,4,5-tetrahydro-1H-pyrrolo[3,2-c]quinoline-1,3a(2H,9bH)-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

2: iron; acetic acid / 5 h / 80 °C

With iron; sodium hydride; acetic acid; In tetrahydrofuran; mineral oil;
DOI:10.1039/c3ob27472a

Reference yield:

: 17422-56-9
diethyl 2-(2-nitrobenzylidene)malonate

: 1426301-91-8
1-benzyl 3a-ethyl 4-oxo-3,3a,4,5-tetrahydro-1H-pyrrolo[3,2-c]quinoline-1,3a(2H,9bH)-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

2: iron; acetic acid / 5 h / 80 °C

With iron; sodium hydride; acetic acid; In tetrahydrofuran; mineral oil;
DOI:10.1039/c3ob27472a