8-[(1S,5R,6S)-6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one

Base Information

• Chemical Name: 8-[(1S,5R,6S)-6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one
• CAS No.: 75629-26-4
• Molecular Formula: C₄₈H₅₂O₁₁
• Molecular Weight: 804.934

Synonyms:8-[(1S,5R,6S)-6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one

Chemical Property of 8-[(1S,5R,6S)-6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 8-[(1S,5R,6S)-6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one

There total 3 articles about 8-[(1S,5R,6S)-6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

RL334 (79004-62-9) + (E)-2-(2,4-dimethoxyphenyl)-5,7-dimethoxy-3-(3-methylbut-2-en-1-yl)-8-(3-methylbuta-1,3-dien-1-yl)-4H-chromen-4-one (79004-61-8) → 8-[(1R,5R,6S)-6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one (79056-25-0) + 8-[(1S,5R,6S)-6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one (75629-26-4)

Guidance literature:

With 2,6-di-tert-butyl-4-methyl-phenol; In toluene; for 81h; Heating;

DOI:10.1016/S0040-4039(01)90496-4

Reference yield:

8-[(1S,5R,6S)-6-(2,4dDihydroxybenzoyl)-5-(2,4-dihydroxyphenyl)-3-methyl-2-cyclohexen-1-yl]-2-(2,4-dihydroxyphenyl)-5,7-dihydroxy-3-(3-methyl-2-buten-1-yl)-4H-chromen-4-one (79056-24-9,75629-19-5) + dimethyl sulfate (77-78-1) → 8-[(1S,5R,6S)-6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one (75629-26-4)

Guidance literature:

With perhydrodibenzo-18-crown-6; potassium carbonate; In acetone; for 19h; Heating;

DOI:10.1246/cl.1980.1577

Reference yield:

moracenin B (75629-19-5,79056-24-9) + dimethyl sulfate (77-78-1) → 2-(2,4-Dimethoxy-phenyl)-8-[5-(2,4-dimethoxy-phenyl)-6-(2-hydroxy-4-methoxy-benzoyl)-3-methyl-cyclohex-2-enyl]-5-hydroxy-7-methoxy-3-(3-methyl-but-2-enyl)-chromen-4-one (75629-23-1) + 2-(2,4-Dimethoxy-phenyl)-8-[5-(2,4-dimethoxy-phenyl)-6-(2-hydroxy-4-methoxy-benzoyl)-3-methyl-cyclohex-2-enyl]-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one (75629-25-3) + 8-[6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5-hydroxy-7-methoxy-3-(3-methyl-but-2-enyl)-chromen-4-one (75629-24-2) + 8-[6-(2,4-Dimethoxy-benzoyl)-5-(2,4-dimethoxy-phenyl)-3-methyl-cyclohex-2-enyl]-2-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-3-(3-methyl-but-2-enyl)-chromen-4-one (75629-26-4,79056-25-0,79056-27-2)

Guidance literature:

In acetone;

DOI:10.1248/cpb.28.2548

upstream raw materials:

RL334

(E)-2-(2,4-dimethoxyphenyl)-5,7-dimethoxy-3-(3-methylbut-2-en-1-yl)-8-(3-methylbuta-1,3-dien-1-yl)-4H-chromen-4-one

8-[(1S,5R,6S)-6-(2,4dDihydroxybenzoyl)-5-(2,4-dihydroxyphenyl)-3-methyl-2-cyclohexen-1-yl]-2-(2,4-dihydroxyphenyl)-5,7-dihydroxy-3-(3-methyl-2-buten-1-yl)-4H-chromen-4-one

dimethyl sulfate

Downstream raw materials:

tetrahydrokuwanon C tetramethyl ether

RL334

2-(2,4-Dimethoxy-phenyl)-5,7-dimethoxy-8-((E)-3-methyl-buta-1,3-dienyl)-3-(3-methyl-but-2-enyl)-chromen-4-one

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