4-((1S,2R,3S,6R)-1,2,3-Trimethyl-7-oxa-bicyclo[4.1.0]hept-2-yl)-butan-2-ol

Base Information

Chemical Name:4-((1S,2R,3S,6R)-1,2,3-Trimethyl-7-oxa-bicyclo[4.1.0]hept-2-yl)-butan-2-ol
CAS No.:92599-03-6
Molecular Formula:C₁₃H₂₄O₂
Molecular Weight:212.332
Hs Code.:

Synonyms:4-((1S,2R,3S,6R)-1,2,3-Trimethyl-7-oxa-bicyclo[4.1.0]hept-2-yl)-butan-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-((1S,2R,3S,6R)-1,2,3-Trimethyl-7-oxa-bicyclo[4.1.0]hept-2-yl)-butan-2-ol

Chemical Property:

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Technology Process of 4-((1S,2R,3S,6R)-1,2,3-Trimethyl-7-oxa-bicyclo[4.1.0]hept-2-yl)-butan-2-ol

There total 1 articles about 4-((1S,2R,3S,6R)-1,2,3-Trimethyl-7-oxa-bicyclo[4.1.0]hept-2-yl)-butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88855-15-6,127995-73-7
(–)-agelasine F

: 626-95-9
1,4-Pentanediol

: 92599-03-6
4-((1S,2R,3S,6R)-1,2,3-Trimethyl-7-oxa-bicyclo[4.1.0]hept-2-yl)-butan-2-ol

Guidance literature:: With sodium tetrahydroborate; dimethylsulfide; ozone; Yield given. Multistep reaction. Yields of byproduct given; 1) methanol, -78 deg C, 15 min; 2) methanol, 20 deg C, 30 min;
DOI:10.1246/bcsj.59.2495

Reference yield: 84.0%

: 92599-03-6
4-((1S,2R,3S,6R)-1,2,3-Trimethyl-7-oxa-bicyclo[4.1.0]hept-2-yl)-butan-2-ol

: 105026-01-5
(1R,2R,3S)-2-(3-Hydroxy-butyl)-1,2,3-trimethyl-cyclohexanol

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; Ambient temperature;
DOI:10.1246/bcsj.59.2495

Reference yield:

: 92599-03-6
4-((1S,2R,3S,6R)-1,2,3-Trimethyl-7-oxa-bicyclo[4.1.0]hept-2-yl)-butan-2-ol

: 105026-05-9
4-((1R,2S)-1,2-Dimethyl-6-methylene-cyclohexyl)-butan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / lithium triethylhydroborate / tetrahydrofuran / Ambient temperature

2: 88 percent / Et₃N, 4-dimethylaminopyridine / 1 h / Ambient temperature

3: 1) thionyl chloride; 2) water / 1) pyridine, -5 deg C, 15 min; 2) pyridine, diethyl ether

With dmap; thionyl chloride; water; lithium triethylborohydride; triethylamine; In tetrahydrofuran;
DOI:10.1246/bcsj.59.2495