ageline A

Base Information

Chemical Name:ageline A
CAS No.:88855-15-6
Molecular Formula:C₂₆H₄₀N₅*Cl
Molecular Weight:458.09
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ageline A

Chemical Property:

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Technology Process of ageline A

There total 29 articles about ageline A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: C₃₀H₄₇N₅O

: 88855-15-6,127995-73-7
(–)-agelasine F

Guidance literature:: C₃₀H₄₇N₅O; With acetic acid; zinc; In methanol; water; at 75 ℃; for 20h; Inert atmosphere;

With sodium chloride; In methanol; water; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.202000202

Reference yield:

: 127891-09-2
((2E,6E)-7-Bromo-3-methyl-octa-2,6-dienyloxymethyl)-benzene

: 88855-15-6,127995-73-7
ageline A

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) t-BuLi, ZnBr₂ / 2.) PdCl₂dppf (3 molpercent) / 1.) Et₂O, THF

2: Li / liquid ammonia

3: PBr₃, C₅H₅N / liquid ammonia

4: 2.) Zn, H₂O / 1.) MeCONMe₂; 2.) AcOH

With pyridine; water; tert.-butyl lithium; phosphorus tribromide; lithium; zinc dibromide; zinc; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In ammonia;
DOI:10.1016/S0040-4039(01)93906-1

Reference yield:

: 127891-07-0
(5R,6S)-6-(2-Iodo-ethyl)-1,5,6-trimethyl-cyclohexene

: 88855-15-6,127995-73-7
ageline A

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) t-BuLi, ZnBr₂ / 2.) PdCl₂dppf (3 molpercent) / 1.) Et₂O, THF

2: Li / liquid ammonia

3: PBr₃, C₅H₅N / liquid ammonia

4: 2.) Zn, H₂O / 1.) MeCONMe₂; 2.) AcOH

With pyridine; water; tert.-butyl lithium; phosphorus tribromide; lithium; zinc dibromide; zinc; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In ammonia;
DOI:10.1016/S0040-4039(01)93906-1