(4-Dimethylamino-phenyl)-glyoxal

Base Information

• Chemical Name: (4-Dimethylamino-phenyl)-glyoxal
• CAS No.: 73318-77-1
• Molecular Formula: C₁₀H₁₁NO₂
• Molecular Weight: 177.203
• Mol file: 73318-77-1.mol

Synonyms:(4-Dimethylamino-phenyl)-glyoxal

Chemical Property of (4-Dimethylamino-phenyl)-glyoxal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4-Dimethylamino-phenyl)-glyoxal

There total 4 articles about (4-Dimethylamino-phenyl)-glyoxal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4'-dimethylaminoacetophenone (2124-31-4) → (4-Dimethylamino-phenyl)-glyoxal (73318-77-1)

Guidance literature:

With iodine; In dimethyl sulfoxide; at 60 ℃; for 6h;

DOI:10.1016/j.tet.2015.08.058

Reference yield:

4’-dimethylamino-2,2-diethoxyacetophenone (32025-67-5) → (4-Dimethylamino-phenyl)-glyoxal (73318-77-1)

Guidance literature:

With hydrogenchloride;

DOI:10.1021/ja01564a043

Reference yield:

4-bromo-N,N-dimethylaniline (586-77-6) → (4-Dimethylamino-phenyl)-glyoxal (73318-77-1)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium; methyl lithium; diethyl ether / anschliessend Erwaermen mit 1-Diaethoxyacetyl-piperidin

2: concentrated aqueous HCl

With hydrogenchloride; diethyl ether; methyllithium; lithium;

DOI:10.1021/ja01564a043

upstream raw materials:

4’-dimethylamino-2,2-diethoxyacetophenone

4-bromo-N,N-dimethylaniline

4'-dimethylaminoacetophenone

Downstream raw materials:

C₂₀H₂₂N₄O

C₂₁H₂₃N₃O₄

C₂₁H₂₃N₃O₄

C₂₂H₂₄N₂O₇