(4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol

Base Information

• Chemical Name: (4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol
• CAS No.: 911836-47-0
• Molecular Formula: C₃₂H₄₂O₂
• Molecular Weight: 458.684

Synonyms:(4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol

Chemical Property of (4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol

Chemical Property:

Purity/Quality:

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Technology Process of (4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol

There total 3 articles about (4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

[4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone (911836-46-9) → (4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol (911836-47-0)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 1.5h;

DOI:10.1021/ol061505i

Reference yield:

5-tert-Butyl-m-xylene (98-19-1) → (4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol (911836-47-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / aluminum chloride / nitrobenzene / 1 h

2: 96 percent / LiAlH₄ / tetrahydrofuran / 1.5 h / 20 °C

With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; nitrobenzene;

DOI:10.1021/ol061505i

Reference yield:

terephthaloyl chloride (100-20-9) → (4-tert-butyl-2,6-dimethyl-phenyl)-{4-[(4-tert-butyl-2,6-dimethyl-phenyl)-hydroxy-methyl]-phenyl}-methanol (911836-47-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / aluminum chloride / nitrobenzene / 1 h

2: 96 percent / LiAlH₄ / tetrahydrofuran / 1.5 h / 20 °C

With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; nitrobenzene;

DOI:10.1021/ol061505i

upstream raw materials:

[4-(4-tert-butyl-2,6-dimethyl-benzoyl)-phenyl]-(4-tert-butyl-2,6-dimethyl-phenyl)-methanone

5-tert-Butyl-m-xylene

terephthaloyl chloride

Downstream raw materials:

C₃₂H₄₀Br₂

1,4-phenylenebis-[1-(4-tert-butyl-2,6-dimethylphenyl)methanamine]

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