Technology Process of C22H34INO5Si
There total 7 articles about C22H34INO5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
In
dichloromethane;
at 0 - 20 ℃;
for 2.41667h;
DOI:10.1021/ja303204m
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere
2: dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate / dichloromethane / 2.42 h / 0 - 20 °C
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja303204m
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Iodine monochloride / dichloromethane / 0 - 20 °C
2.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 20 - 40 °C / Inert atmosphere
3.1: magnesium / diethyl ether / Reflux
3.2: 20 °C
4.1: dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate / dichloromethane / 2.42 h / 0 - 20 °C
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); Iodine monochloride; magnesium; triethylamine; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
In
diethyl ether; dichloromethane;
DOI:10.1021/ja303204m
