(2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalaninyl benzyl ester hydrochloride

Base Information

Chemical Name:(2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalaninyl benzyl ester hydrochloride
CAS No.:1329063-38-8
Molecular Formula:C₂₅H₂₇N₃O₃*ClH
Molecular Weight:453.969
Hs Code.:

Synonyms:(2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalaninyl benzyl ester hydrochloride

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Chemical Property of (2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalaninyl benzyl ester hydrochloride

Chemical Property:

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Technology Process of (2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalaninyl benzyl ester hydrochloride

There total 6 articles about (2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalaninyl benzyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1329063-37-7
N-Boc-(2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalanine benzyl ester

: 1329063-38-8
(2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalaninyl benzyl ester hydrochloride

Guidance literature:: N-Boc-(2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalanine benzyl ester; With trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In water; for 1h; Inert atmosphere;
DOI:10.1021/jm200608k

Reference yield:

: 1329063-33-3
(3S)-β-homophenylalanine benzyl ester hydrochloride

: 1329063-38-8
(2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalaninyl benzyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

1.2: 3 h / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm200608k

Reference yield:

: 51871-62-6
(S)-3-tert-butoxycarbonylamino-4-phenylbutanoic acid

: 1329063-38-8
(2S)-(3-pyridyl)alaninyl-(3S)-β-homophenylalaninyl benzyl ester hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / water; acetonitrile / 1 h / Inert atmosphere

1.2: Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

3.2: 3 h / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

4.2: 1 h / Inert atmosphere

With benzotriazol-1-ol; caesium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; trifluoroacetic acid; In dichloromethane; water; acetonitrile;
DOI:10.1021/jm200608k