(E)-2-(((4-methoxybenzyl)oxy)methyl)-6,10-dimethylundeca-1,5,10-trien-4-one

Base Information

Chemical Name:(E)-2-(((4-methoxybenzyl)oxy)methyl)-6,10-dimethylundeca-1,5,10-trien-4-one
CAS No.:1432620-60-4
Molecular Formula:C₂₂H₃₀O₃
Molecular Weight:342.478
Hs Code.:

Synonyms:(E)-2-(((4-methoxybenzyl)oxy)methyl)-6,10-dimethylundeca-1,5,10-trien-4-one

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Chemical Property of (E)-2-(((4-methoxybenzyl)oxy)methyl)-6,10-dimethylundeca-1,5,10-trien-4-one

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Technology Process of (E)-2-(((4-methoxybenzyl)oxy)methyl)-6,10-dimethylundeca-1,5,10-trien-4-one

There total 5 articles about (E)-2-(((4-methoxybenzyl)oxy)methyl)-6,10-dimethylundeca-1,5,10-trien-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1432620-57-9
(E)-N-Methoxy-N,3,7-trimethylocta-2,7-dienamide

: 454482-62-3
1-(((2-(chloromethyl)allyl)oxy)methyl)-4-methoxybenzene

: 1432620-60-4
(E)-2-(((4-methoxybenzyl)oxy)methyl)-6,10-dimethylundeca-1,5,10-trien-4-one

Guidance literature:: 1-(((2-(chloromethyl)allyl)oxy)methyl)-4-methoxybenzene; With magnesium; ethylene dibromide; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

(E)-N-Methoxy-N,3,7-trimethylocta-2,7-dienamide; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c3ob40120k

Reference yield:

: 20038-12-4
4-bromo-2-methylbut-1-ene

: 1432620-60-4
(E)-2-(((4-methoxybenzyl)oxy)methyl)-6,10-dimethylundeca-1,5,10-trien-4-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

2.1: lithium hydroxide / water

3.1: copper(l) cyanide / diethyl ether

4.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h

5.1: magnesium; ethylene dibromide / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

5.2: 0.5 h / -78 °C / Inert atmosphere

With isopropylmagnesium chloride; copper(l) cyanide; magnesium; ethylene dibromide; lithium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; water;
DOI:10.1039/c3ob40120k

Reference yield:

: 110995-23-8
ethyl 7-methyl-3-oxo-7-octenate

: 1432620-60-4
(E)-2-(((4-methoxybenzyl)oxy)methyl)-6,10-dimethylundeca-1,5,10-trien-4-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hydroxide / water

2.1: copper(l) cyanide / diethyl ether

3.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h

4.1: magnesium; ethylene dibromide / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

4.2: 0.5 h / -78 °C / Inert atmosphere

With isopropylmagnesium chloride; copper(l) cyanide; magnesium; ethylene dibromide; lithium hydroxide; In tetrahydrofuran; diethyl ether; water;
DOI:10.1039/c3ob40120k