C₂₁H₃₃NO₄Si

Base Information

Chemical Name:C₂₁H₃₃NO₄Si
CAS No.:1353545-65-9
Molecular Formula:C₂₁H₃₃NO₄Si
Molecular Weight:391.583
Hs Code.:

C<sub>21</sub>H<sub>33</sub>NO<sub>4</sub>Si

Synonyms:C₂₁H₃₃NO₄Si

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Chemical Property of C₂₁H₃₃NO₄Si

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Technology Process of C₂₁H₃₃NO₄Si

There total 2 articles about C₂₁H₃₃NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: C₂₁H₃₁NO₄Si

: 1353545-65-9
C₂₁H₃₃NO₄Si

Guidance literature:: With copper(l) iodide; methyllithium; diisobutylaluminium hydride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; cyclohexane; at -78 ℃; for 1.16667h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.11.038

Reference yield:

: 89922-82-7
3-(tert-butyldimethylsilanyloxy)propionaldehyde

: 204587-88-2
[2-((R)-4-benzyl-2-oxooxazolidin-3-yl)-2-oxoethyl]phosphonic acid diethyl ester

: 1353545-65-9
C₂₁H₃₃NO₄Si

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; lithium chloride / acetonitrile / 4 h / Cooling with ice

2: copper(l) iodide; methyllithium; diisobutylaluminium hydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; cyclohexane / 1.17 h / -78 °C / Inert atmosphere

With copper(l) iodide; methyllithium; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; cyclohexane; acetonitrile; 1: Wittig-Horner reaction;
DOI:10.1016/j.tet.2011.11.038