2-(2-bromo-acetoxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

Base Information

Chemical Name:2-(2-bromo-acetoxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester
CAS No.:1240261-46-4
Molecular Formula:C₁₅H₁₆BrNO₉
Molecular Weight:434.197
Hs Code.:

Synonyms:2-(2-bromo-acetoxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

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Chemical Property of 2-(2-bromo-acetoxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

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Technology Process of 2-(2-bromo-acetoxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

There total 4 articles about 2-(2-bromo-acetoxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1240261-43-1
2-hydroxy-benzoic acid benzyloxy carbonyl methyl ester

: 1240261-46-4
2-(2-bromo-acetoxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h

2: triethylamine / acetone / 16 h / 40 °C

3: silver nitrate / acetonitrile / 8 h / 50 °C

4: pyridine / dichloromethane / 2 h / 0 - 5 °C / Inert atmosphere

With pyridine; hydrogen; silver nitrate; triethylamine; palladium 10% on activated carbon; In dichloromethane; ethyl acetate; acetone; acetonitrile;

Reference yield:

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 1240261-46-4
2-(2-bromo-acetoxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / acetone / 4 h / 50 °C

2: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h

3: triethylamine / acetone / 16 h / 40 °C

4: silver nitrate / acetonitrile / 8 h / 50 °C

5: pyridine / dichloromethane / 2 h / 0 - 5 °C / Inert atmosphere

With pyridine; hydrogen; silver nitrate; triethylamine; palladium 10% on activated carbon; In dichloromethane; ethyl acetate; acetone; acetonitrile;

Reference yield:

: 108085-52-5
salicyloyloxy-acetic acid

: 1240261-46-4
2-(2-bromo-acetoxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / acetone / 16 h / 40 °C

2: silver nitrate / acetonitrile / 8 h / 50 °C

3: pyridine / dichloromethane / 2 h / 0 - 5 °C / Inert atmosphere

With pyridine; silver nitrate; triethylamine; In dichloromethane; acetone; acetonitrile;